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CAS RN: 90916-29-3 | Product Number: A1632

N-Allyloxycarbonyl-2-nitrobenzenesulfonamide


Purity: >98.0%(N)
Synonyms:
  • N-Alloc-2-nitrobenzenesulfonamide
Documents:
5G
$263.00
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Product Number A1632
Purity / Analysis Method >98.0%(N)
Molecular Formula / Molecular Weight C__1__0H__1__0N__2O__6S = 286.26  
Physical State (20 deg.C) Solid
CAS RN 90916-29-3
Reaxys Registry Number 2764631
PubChem Substance ID 87563065
MDL Number

MFCD06797039

Specifications
Appearance White to Almost white powder to crystal
Purity(HPLC) min. 95.0 area%
Purity(with Total Nitrogen) min. 98.0 %
Melting point 103.0 to 107.0 °C
Properties (reference)
Melting Point 105 °C
Solubility (soluble in) Methanol
GHS
Pictogram Pictogram
Signal Word Warning
Hazard Statements H315 : Causes skin irritation.
H319 : Causes serious eye irritation.
Precautionary Statements P264 : Wash skin thoroughly after handling.
P280 : Wear protective gloves/ eye protection/ face protection.
P337 + P313 : If eye irritation persists: Get medical advice/ attention.
P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P302 + P352 : IF ON SKIN: Wash with plenty of soap and water.
P332 + P313 : If skin irritation occurs: Get medical advice/ attention.
P362 : Take off contaminated clothing and wash before reuse.
Related Laws:
Transport Information:
HS Number 2935.90.9500
Application
Aminating Agent

Experimental procedure: To a stirred solution of 1 (289 mg, 1.01 mmol), L-ethyl lactate (228 µL, 2.01 mmol) and triphenylphosphine (528 mg, 2.01 mmol) in benzene (3 mL) is slowly added diethyl azodicarboxylate (2.01 mmol) of at room temperature under argon. After 30 min the reaction mixture is concentrated in vacuo and the residue is purified by chromatography on silica gel (CH2Cl2 : hexanes) to give 2 (93% yield).

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