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CAS RN: 16308-68-2 | Product Number: A2303

Allyl Phenyl Carbonate


Purity: >97.0%(GC)
Synonyms:
  • Carbonic Acid Allyl Phenyl Ester
Documents:
5G
$72.00
4   1   Contact Us
25G
$209.00
8   1   12  

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Product Number A2303
Purity / Analysis Method >97.0%(GC)
Molecular Formula / Molecular Weight C__1__0H__1__0O__3 = 178.19  
Physical State (20 deg.C) Liquid
Store Under Inert Gas Store under inert gas
Condition to Avoid Air Sensitive
CAS RN 16308-68-2
Reaxys Registry Number 3253031
PubChem Substance ID 125307508
MDL Number

MFCD07784342

Specifications
Appearance Colorless to Almost colorless clear liquid
Purity(GC) min. 97.0 %
Properties (reference)
Boiling Point 78 °C/0.2 mmHg
Specific Gravity (20/20) 1.11
Refractive Index 1.50
GHS
Pictogram Pictogram
Signal Word Warning
Hazard Statements H319 : Causes serious eye irritation.
Precautionary Statements P264 : Wash skin thoroughly after handling.
P280 : Wear eye protection/ face protection.
P337 + P313 : If eye irritation persists: Get medical advice/ attention.
P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
Related Laws:
Transport Information:
HS Number 2916.39.7900
Application
Mono Carbamate Protection of Aliphatic Diamines

Typical Procedure (Mono Carbamate Protection of Aliphatic Diamines): Allyl phenyl carbonate (10 mmol) is added to a stirring solution of diamine (5.0 mmol) in absolute EtOH (20 mL). The reaction mixture is stirred over night at room temperature followed by removal of the volatiles in vacuo. H2O (25 mL) is added and the pH adjusted to 3 by addition of aq. HCl (2 M) followed by extraction with CH2Cl2 (2 × 50 mL). The aq phase is then made strongly alkaline by addition of aq. NaOH (2 M) and extracted with CH2Cl2 (3 × 80 mL). The organic phase is dried (Na2SO4), filtered and concentrated in vacuo to afford the desired products.

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