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CAS RN: 1580548-81-7 | Product Number: A2678


Purity: >97.0%(T)
  • ABBX
2   1  

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Product Number A2678
Purity / Analysis Method >97.0%(T)
Molecular Formula / Molecular Weight C__9H__6BrIO__4 = 384.95  
Physical State (20 deg.C) Solid
Store Under Inert Gas Store under inert gas
Condition to Avoid Moisture Sensitive
CAS RN 1580548-81-7
PubChem Substance ID 253661571
Appearance White to Light yellow powder to crystal
Purity(Iodometric Titration) min. 97.0 %
Properties (reference)
Pictogram Pictogram
Signal Word Warning
Hazard Statements H315 : Causes skin irritation.
H319 : Causes serious eye irritation.
Precautionary Statements P264 : Wash skin thoroughly after handling.
P280 : Wear protective gloves/ eye protection/ face protection.
P302 + P352 : IF ON SKIN: Wash with plenty of water.
P337 + P313 : If eye irritation persists: Get medical advice/ attention.
P362 + P364 : Take off contaminated clothing and wash it before reuse.
P332 + P313 : If skin irritation occurs: Get medical advice/ attention.
Related Laws:
Transport Information:
HS Number 2934999090
Oxidation of alcohols to aldehydes or ketones with a new highly active trivalent iodine compound, ABBX


Typical Procedure (oxidation of 4-methylbenzyl alcohol to 4-methylbenzaldehyde): To a solution of 4-methylbenzyl alcohol (1.0 mmol, 122.1 mg) in CHCl3 (4 mL) is added ABBX (2.0 mmol, 767.7 mg). The mixture is stirred at 60 °C for 24 h. After the reaction is completed, the reaction mixture is added to aq. NaHCO3 (10 mL). The aqueous layer is extracted with CHCl3 (3 × 10 mL), and the organic layer is dried over Na2SO4. The filtrate is concentrated under reduced pressure to give 4-methylbenzaldehyde (108.0 mg, 90% yield) with 90% purity. The aqueous layer is acidified (pH ca. 2) with 1 M aq. HCl (15 mL) and the obtained mixture is filtered to afford 2-iodo-5-bromobenzoic acid (593 mg, 91%).


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