CAS RN: 6046-93-1 | Product Number: C2346
Copper(II) Acetate Monohydrate
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|Appearance||Blue to Dark blue powder to crystal|
|Purity(Chelometric Titration)||min. 95.0 %|
|Melting Point||115 °C|
|Solubility in water||Soluble|
|Solubility (soluble in)||Alcohol|
|Solubility (slightly sol. in)||Ether|
|Hazard Statements||H302 : Harmful if swallowed.
H411 : Toxic to aquatic life with long lasting effects.
|Precautionary Statements||P501 : Dispose of contents/ container to an approved waste disposal plant.
P273 : Avoid release to the environment.
P270 : Do not eat, drink or smoke when using this product.
P264 : Wash skin thoroughly after handling.
P391 : Collect spillage.
P301 + P312 + P330 : IF SWALLOWED: Call a POISON CENTER/doctor if you feel unwell. Rinse mouth.
To a 20 mL two-necked flask with a reflux condenser and a rubber cap are added 2-aminobiphenyls (0.5 mmol), [Cp*IrCl2]2 (0.01 mmol, 8.0 mg), Cu(OAc)2 (0.1 mmol, 18 mg), pivalic acid (1 mmol, 102 mg), 1-methylnaphthalene (ca. 30 mg) as an internal standard, and N-methyl-2-pyrrolidone (NMP, 3 mL). Then, the resulting mixture is stirred under air at 120 °C for 3-6 h. After cooling, the reaction mixture is extracted with ethyl acetate (100 mL). The organic layer is washed by aqueous NaHCO3 (100 mL×3), and dried over Na2SO4. After evaporation of the solvents under vacuum, the product is isolated by column chromatography on silica gel using hexane-ethyl acetate (10:1) as the eluent.
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