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CAS RN: 1068-21-9 | Product Number: D2361

Diethyl Phosphoramidate


Purity: >98.0%(GC)
Synonyms:
  • Diethyl Amidophosphate
  • Diethyl Phosphoryl Amide
Documents:
5G
€28.00
2   12  
25G
€109.00
4   2  

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Product Number D2361
Purity / Analysis Method >98.0%(GC)
Molecular Formula / Molecular Weight C__4H__1__2NO__3P = 153.12 
Physical State (20 deg.C) Solid
Store Under Inert Gas Store under inert gas
Condition to Avoid Moisture Sensitive
CAS RN 1068-21-9
Reaxys Registry Number 1704111
PubChem Substance ID 87568797
MDL Number

MFCD00015676

Specifications
Appearance White to Light yellow to Light orange powder to crystal
Purity(GC) min. 98.0 %
Melting point 50.0 to 55.0 °C
Properties (reference)
Melting Point 52 °C
Boiling Point 140 °C/3 mmHg
GHS
Pictogram Pictogram
Signal Word Warning
Hazard Statements H302 + H312 + H332 : Harmful if swallowed, in contact with skin or if inhaled.
H315 : Causes skin irritation.
H319 : Causes serious eye irritation.
Precautionary Statements P261 : Avoid breathing dust/ fume/ gas/ mist/ vapours/ spray.
P264 : Wash skin thoroughly after handling.
P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection.
P337 + P313 : If eye irritation persists: Get medical advice/ attention.
P302 + P352 + P312 : IF ON SKIN: Wash with plenty of water. Call a POISON CENTER/doctor if you feel unwell.
P304 + P340 + P312 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Call a POISON CENTER/doctor if you feel unwell.
Related Laws:
Transport Information:
HS Number 2929900090
Application
Aminating Agent

Experimental procedure: A microwave tube is charged with 1 (0.137 mmol), Pd2(dba)3 (8 mg, 6 mol%), (±)-BINAP (11 mg, 12 mol%) and Cs2CO3 (0.343 mmol). The vessel is sealed with a septum and purged with argon. Degassed 1,4-dioxane (1.7 mL) and diethyl phosphoramidate (0.206 mmol) are introduced through the septum. The resulting mixture is heated by using a microwave apparatus to 130 °C for 1 h. After cooling, the reaction mixture is concentrated and purified by column chromatography to give 2 (44 mg, 87% yield) as a pale white solid.

References


PubMed Literature


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