CAS RN: 2902-68-3 | Product Number: I0865
*Stock available in Belgium will be delivered in 1 to 3 days
*Stock available in Japan will be delivered in 1 to 2 weeks (excludes regulated items and dry ice shipments).
|Appearance||White to Almost white powder to crystal|
|Purity(Iodometric Titration)||min. 98.0 %|
|Melting Point||263 °C|
|Hazard Statements||H315 : Causes skin irritation.
H319 : Causes serious eye irritation.
|Precautionary Statements||P264 : Wash skin thoroughly after handling.
P280 : Wear protective gloves/ eye protection/ face protection.
P302 + P352 : IF ON SKIN: Wash with plenty of water.
P337 + P313 : If eye irritation persists: Get medical advice/ attention.
P362 + P364 : Take off contaminated clothing and wash it before reuse.
P332 + P313 : If skin irritation occurs: Get medical advice/ attention.
The aqueous layer is acidified with 5 N HCl (pH < 7), and most of water is removed in vacuo to give the crude material. Conc. HCl (15 mL) is poured into the residue, and aq. 5.8% NaOCl soln. (35 mL) is added dropwise to the vigorously stirred mixture at room temperature. After the addition of NaOCl is complete, stirring is continued for a further 4 h. The precipitated white solid is collected by filtration, washed with H2O, diethyl ether, and acetone, and dried at room temperature to give 1.63 g of iodosodilactone in 94% recovery yield.
- Recyclable Hypervalent Iodine(III) Reagent Iodosodilactone as an Efficient Coupling Reagent for Direct Esterification, Amidation, and Peptide Coupling
Safety Data Sheet (SDS)
The requested SDS is not available.
Please Contact Us for more information.
C of A & Other Certificates
The requested analytical chart is not available. Sorry for the inconvenience.