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CAS RN: 68123-33-1 | Product Number: A5522
N-Succinimidyl 4-Nitrophenylacetate [for HPLC Labeling]
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|Purity / Analysis Method||>98.0%(N)|
|Molecular Formula / Molecular Weight||C__1__2H__1__0N__2O__6 = 278.22|
|Physical State (20 deg.C)||Solid|
|Store Under Inert Gas||Store under inert gas|
|Condition to Avoid||Moisture Sensitive,Heat Sensitive|
|Reaxys Registry Number||6228910|
|PubChem Substance ID||87563163|
|SDBS (AIST Spectral DB)||11057|
|Appearance||White to Almost white powder to crystal|
|Purity(with Total Nitrogen)||min. 98.0 %|
|Melting point||181.0 to 185.0 °C|
|Solubility in hot Acetone||almost transparency|
|Effect test of HPLC derivatization||Effective as labeling agent for Ｄiethylamine.|
|Melting Point||181 °C|
|Hazard Statements||H315 : Causes skin irritation.
H319 : Causes serious eye irritation.
|Precautionary Statements||P264 : Wash skin thoroughly after handling.
P280 : Wear protective gloves/ eye protection/ face protection.
P302 + P352 : IF ON SKIN: Wash with plenty of water.
P337 + P313 : If eye irritation persists: Get medical advice/ attention.
P362 + P364 : Take off contaminated clothing and wash it before reuse.
P332 + P313 : If skin irritation occurs: Get medical advice/ attention.
1~5 mg of a sample (free amine), 5 mL of THF, and 50 mg of labeling reagent 1 are mixed, and incubated at 60°C for 1 h. After cooling to room temperature, use it as an HPLC sample. If it is necessary to remove the unreacted labeling reagent and by-product, N-hydroxysuccinimide, evaporate the solvent at a low temperature under a nitrogen atmosphere. Dissolve the residue in 2~3 mL of ether and wash with aqueous NaHCO3 and water.
Drugs (amphetamine, methamphetamine)1)
HPLC Labeling Reagents ( PDF 10MB )
- 1)T. H. Jupille, Am. Lab. 1976, 8, 85.
Safety Data Sheet (SDS)
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C of A & Other Certificates
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