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CAS RN: 830-74-0 | Product Number: A2943

1-Allylisatin


Purity: >98.0%(GC)
Synonyms:
  • 1-Allylindole-2,3-dione
  • 1-Allyl-2,3-indolinedione
Documents:
1G
€110.00
2   ≥20 

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Product Number A2943
Purity / Analysis Method >98.0%(GC)
Molecular Formula / Molecular Weight C__1__1H__9NO__2 = 187.2  
Physical State (20 deg.C) Solid
CAS RN 830-74-0
Reaxys Registry Number 1528099
PubChem Substance ID 354333758
MDL Number

MFCD00224218

Specifications
Properties (reference)
Melting Point 86 °C
Boiling Point 145 °C/1 mmHg
Maximum Absorption Wavelength 267 nm
GHS
Pictogram Pictogram
Signal Word Warning
Hazard Statements H315 : Causes skin irritation.
H319 : Causes serious eye irritation.
Precautionary Statements P264 : Wash skin thoroughly after handling.
P280 : Wear protective gloves/ eye protection/ face protection.
P302 + P352 : IF ON SKIN: Wash with plenty of water.
P337 + P313 : If eye irritation persists: Get medical advice/ attention.
P362 + P364 : Take off contaminated clothing and wash it before reuse.
P332 + P313 : If skin irritation occurs: Get medical advice/ attention.
Related Laws: / Compliance with laws, Regulations
Transport Information:
HS Number 2933790090
Application
Multicomponent Reactions involving Arynes, Heterocycles, and Isatins

Experimental procedure: To a screw-capped test tube equipped is added 18-crown 6-ether (0.396 g, 1.5 mmol), KF (0.087 g, 1.5 mmol) and 1 (0.094 g, 0.50 mmol). Then the tube is evacuated and backfilled with argon. The mixture is dissolved in THF (2.0 mL). The resultant reaction mixture is kept stirring at 30 °C for 5 min. To the stirring solution is added pyridine (0.060 g, 0.75 mmol) and the 2-(trimethylsilyl)phenyl trifluoromethane sulfonate (0.223 g, 0.75 mmol) and the reaction mixture is stirred for 12 h at 30 °C. The reaction stops and the crude reaction mixture is purified by column chromatography (Pet. ether:EtOAc = 75 : 25) on silica gel to afford 2 (0.126 g, 73%) as a yellow solid.

References


PubMed Literature


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