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CAS RN: 5807-14-7 | Product Number: T1982
1,5,7-Triazabicyclo[4.4.0]dec-5-ene
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![1,5,7-Triazabicyclo[4.4.0]dec-5-ene](/_ui/responsive/theme-tci/images/missing_product_zoom.jpg "1,5,7-Triazabicyclo[4.4.0]dec-5-ene")
Purity: >98.0%(T)(HPLC)
Synonyms:
- 1,3,4,6,7,8-Hexahydro-2H-pyrimido[1,2-a]pyrimidine
- TBD
Product Documents:
| Size | Unit Price | Same Day | 2-3 Business Days | Other Lead Time |
Shipping Information
|
|---|---|---|---|---|---|
| 5G |
$85.00
|
31 | ≥100 | It can be shipped in about 1 week after ordering | |
| 25G |
$290.00
|
12 | ≥100 | Contact Us |
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* The storage conditions are subject to change without notice.
| Product Number | T1982 |
| Purity / Analysis Method | >98.0%(T)(HPLC) |
| Molecular Formula / Molecular Weight | C__7H__1__3N__3 = 139.20 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
| Store Under Inert Gas | Store under inert gas |
| Condition to Avoid | Moisture Sensitive |
| CAS RN | 5807-14-7 |
| Reaxys Registry Number | 3242 |
| PubChem Substance ID | 125307356 |
| MDL Number | MFCD00043003 |
Specifications
| Appearance | White to Almost white powder to crystal |
| Purity(HPLC) | min. 98.0 area% |
| Purity(Nonaqueous Titration) | min. 98.0 % |
| Melting point | 128.0 to 133.0 °C |
Properties (reference)
| Melting Point | 130 °C |
GHS
| Pictogram |
|
| Signal Word | Danger |
| Hazard Statements | H314 : Causes severe skin burns and eye damage. |
| Precautionary Statements | P501 : Dispose of contents/ container to an approved waste disposal plant. P260 : Do not breathe dusts or mists. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection. P303 + P361 + P353 : IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water/shower. P301 + P330 + P331 : IF SWALLOWED: Rinse mouth. Do NOT induce vomiting. P363 : Wash contaminated clothing before reuse. P304 + P340 + P310 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Immediately call a POISON CENTER/doctor. P305 + P351 + P338 + P310 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER/doctor. P405 : Store locked up. |
Related Laws:
Transport Information:
| UN Number | UN3263 |
| Class | 8 |
| Packing Group | II |
| H.S.code* | 2933.99-000 |
Application
TBD-organocatalysed synthesis of pyrazolines
Typical procedure (solvent: CH3CN): Chalcone (214.5 mg), acetylhydrazine (98.8 mg, 1.2 eq.) and TBD (13.9 mg, 0.1 eq.) are introduced into a Schlenk tube under nitrogen. Then, anhydrous CH3CN (1 mL) is added at room temperature and the solution is heated at 60 °C for 24 h. The reaction mixture is allowed to stand at room temperature and concentrated in vacuo. The residue is purified by flash column chromatography (eluent: EtOAc/petroleum ether = 2:3) to give 1-acetyl-3,5-diphenyl-4,5-dihydro-1H-pyrazole as a white powder (216.4 mg, 82 %).
References
Application
Strong Organic Bases
References
- 1)Basicity scale in acetonitrile
- 2)Total synthesis of Ustiloxin D
- 3)Wittig and Horner?Emmons reactions
PubMed Literature
Articles/Brochures
TCIMAIL
[TCIMAIL No.150] Strong Organic Bases[Product Highlights] TBD-Organocatalysed Synthesis of Pyrazolines
Product Documents (Note: Some products will not have analytical charts available.)
Safety Data Sheet (SDS)
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Specifications
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