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CAS RN: 851030-18-7 | Product Number: B4587


Purity: >95.0%(T)(HPLC)
  • DBT-Cl
1   ≥20 
1   ≥20 

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Product Number B4587
Purity / Analysis Method >95.0%(T)(HPLC)
Molecular Formula / Molecular Weight C__1__7H__1__4ClN__3O__2 = 327.77  
Physical State (20 deg.C) Solid
CAS RN 851030-18-7
Reaxys Registry Number 15462339
PubChem Substance ID 354333516
Appearance White to Almost white powder to crystal
Purity(HPLC) min. 95.0 area%
Purity(Argentmetric Titration) min. 95.0 %
Melting point 64.0 to 68.0 °C
Properties (reference)
Melting Point 66 °C
Pictogram Pictogram
Signal Word Warning
Hazard Statements H315 : Causes skin irritation.
H319 : Causes serious eye irritation.
Precautionary Statements P264 : Wash skin thoroughly after handling.
P280 : Wear protective gloves/ eye protection/ face protection.
P302 + P352 : IF ON SKIN: Wash with plenty of water.
P337 + P313 : If eye irritation persists: Get medical advice/ attention.
P362 + P364 : Take off contaminated clothing and wash it before reuse.
P332 + P313 : If skin irritation occurs: Get medical advice/ attention.
Related Laws: / Compliance with laws, Regulations
Transport Information:
HS Number 2933698090
A Triazine Derivative Usable for the Glycosylation Reaction of Unprotected Sugars


Experimental procedure1): 2,4-bis(benzyloxy)-6-chloro-1,3,5-triazine (1, 12.3 g, 37.5 mmol) is added to a solution of D-glucose (4.5 g, 25 mmol), N-methylmorpholine (4.1 mL, 38 mmol) and ammonia (3.3 mL, 50 mmol, 29% aqueous solution) in the mixture of acetonitrile and water (125 mL, CH3CN:H2O = 1:1) and the resulting mixture is stirred for 3 h at 0 °C. After concentration in vacuo, the residue is washed with water and chloroform. The filtrate is concentrated in vacuo to give β-glucoside (9.42 g, 20.0 mmol, 80 % yield).
  Excess amount of alcohol is added to the mixture of β-glucoside (0.2 mmol) and Pd/C (5 mg). Under hydrogen atmosphere, the resulting mixture is stirred at room temperature. The reaction mixture is filtered, and the filtrate is concentrated in vacuo to afford the alkoxy group substituted glucosides.


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