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Published TCIMAIL newest issue No.201
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CAS RN: 1068-21-9 | Product Number: D2361
Diethyl Phosphoramidate
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Purity: >98.0%(GC)
Synonyms:
- Diethyl Amidophosphate
- Diethyl Phosphoryl Amide
Product Documents:
| Size | Unit Price | Belgium | Japan* |
Shipping Information
|
|---|---|---|---|---|
| 5G |
28,00 €
|
Ships within 3 weeks after ordering | 22 | |
| 25G |
109,00 €
|
5 | 2 |
* Stock available in Belgium: Shipment on the same day
* Stock available in Japan: Please check the Shipping Simulation for estimated shipments. (excludes regulated items and dry ice shipments)
| Product Number | D2361 |
Purity / Analysis Method 
|
>98.0%(GC) |
| Molecular Formula / Molecular Weight | C__4H__1__2NO__3P = 153.12 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature
|
Room Temperature (Recommended in a cool and dark place, <15°C) |
| Store Under Inert Gas | Store under inert gas |
| Condition to Avoid | Moisture Sensitive |
| CAS RN | 1068-21-9 |
| Reaxys Registry Number | 1704111 |
| PubChem Substance ID | 87568797 |
| MDL Number | MFCD00015676 |
Specifications
| Appearance | White to Light yellow to Light orange powder to crystal |
| Purity(GC) | min. 98.0 % |
| Melting point | 50.0 to 55.0 °C |
Properties (reference)
| Melting Point | 52 °C |
| Boiling Point | 140 °C/3 mmHg |
GHS
| Pictogram |
|
| Signal Word | Warning |
| Hazard Statements | H302 + H312 + H332 : Harmful if swallowed, in contact with skin or if inhaled. H315 : Causes skin irritation. H319 : Causes serious eye irritation. |
| Precautionary Statements | P261 : Avoid breathing dust. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection/ hearing protection. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P302 + P352 + P312 : IF ON SKIN: Wash with plenty of water. Call a POISON CENTER/doctor if you feel unwell. P304 + P340 + P312 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Call a POISON CENTER/doctor if you feel unwell. |
Related Laws:
Transport Information:
| HS Number | 2929909090 |
Application
Aminating Agent
Experimental procedure: A microwave tube is charged with 1 (0.137 mmol), Pd2(dba)3 (8 mg, 6 mol%), (±)-BINAP (11 mg, 12 mol%) and Cs2CO3 (0.343 mmol). The vessel is sealed with a septum and purged with argon. Degassed 1,4-dioxane (1.7 mL) and diethyl phosphoramidate (0.206 mmol) are introduced through the septum. The resulting mixture is heated by using a microwave apparatus to 130 °C for 1 h. After cooling, the reaction mixture is concentrated and purified by column chromatography to give 2 (44 mg, 87% yield) as a pale white solid.
References
- Buchwald–Hartwig Amination Approach for the Synthesis of Functionalized 1,2,3,4-Tetrahydroacridine Derivatives
PubMed Literature
Product Documents (Note: Some products will not have analytical charts available.)
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