CAS RN: 205319-10-4 | Product Number: D4333
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|Purity / Analysis Method||>98.0%(T)|
|Molecular Formula / Molecular Weight||C__3__9H__3__2Cl__2OP__2Pd = 755.95|
|Physical State (20 deg.C)||Solid|
|Store Under Inert Gas||Store under inert gas|
|Condition to Avoid||Air Sensitive|
|Reaxys Registry Number||17620547|
|PubChem Substance ID||253659676|
|Appearance||Light yellow to Brown powder to crystal|
|Purity(Chelometric Titration)||min. 97.0 %|
|Melting Point||287 °C(dec.)|
A mixture of Pd(Xantphos)Cl2 (7.6 mg, 5 mol %), toluene derivative (20.0 mmol), amine (0.2 mmol) and TBP (53.0 mg, 0.36 mmol) is added into an autoclave. Then the autoclave is purged and charged with CO at 10 atm. The reaction mixture is stirred at 120 °C for 16 h, and then CO is carefully released. The corresponding reaction mixture is purified by flash column chromatography on silica gel to give the desired product.
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