CAS RN: 15956-28-2 | Product Number: R0069
Rhodium(II) Acetate Dimer
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|Appearance||Green to Dark green powder to crystal|
|Elemental analysis(Carbon)||20.50 to 22.70 %|
|Melting Point||240 °C|
Alkyne (0.2 mmol), TsN3 (1.0 eq.), alkenyl alkyl ether (3.0 eq.), CuTC (10.0 mol%), Rh2(OAc)4 (1.0 mol%), and DCE (0.2 M) are added to an oven-dried test tube under nitrogen atmosphere. The reaction mixture is stirred at ambient temperature for 3 h and then, heated at 80 °C for 4–13 h. After the reaction mixture is filtered through short path of celite with CH2Cl2, the filtrate is concentrated under reduced pressure. The residue is purified by silica gel column chromatography (ethyl acetate–hexane) to give pyrrole derivatives (Y. 65–81%).
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