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CAS RN: 73482-96-9 | Product Number: R0161

Rhodium(II) Octanoate Dimer


Purity:
Synonyms:
  • Tetrakis(octanoato)dirhodium(II)
Documents:
200MG
€63.00
5   5  
1G
€218.00
2   8  

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Product Number R0161
Molecular Formula / Molecular Weight C__3__2H__6__0O__8Rh__2 = 778.64  
Physical State (20 deg.C) Solid
CAS RN 73482-96-9
Reaxys Registry Number 14206645
PubChem Substance ID 253662547
MDL Number

MFCD00064724

Specifications
Appearance Green to Dark green powder to crystal
Elemental analysis(Carbon) 47.00 to 52.00 %
Properties (reference)
GHS
Related Laws: / Compliance with laws, Regulations
Transport Information:
HS Number 2843909000
Application
An Intramolecular C-H Amination of Aryl Azides

Experimental procedure: to a mixture of 1 (0.056 g, 0.246 mmol), Rh2(O2CC7H15)4 (0.012 mmol) and 4A molecular sieves (0.056 g) is added 1,2-dichloroethane (0.2 mL). The resulting mixture is heated to 60 °C. After 16 h, the reaction mixture is cooled to room temperature, and the heterogenous mixture is filtered through SiO2. The filtrate is concentrated in vacuo. Purification by MPLC (EtOAc:hexanes = 0:100 – 5:95) affords 2 (0.034 g, 69% yield) as a white solid.

References


PubMed Literature


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