CAS RN: 34946-82-2 | Product Number: T1292
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|Purity / Analysis Method||>98.0%(T)|
|Molecular Formula / Molecular Weight||C__2CuF__6O__6S__2 = 361.67|
|Physical State (20 deg.C)||Solid|
|Store Under Inert Gas||Store under inert gas|
|Condition to Avoid||Hygroscopic|
|Reaxys Registry Number||4028198|
|PubChem Substance ID||87577063|
|Appearance||White to Gray to Dark blue powder to crystal|
|Purity(Chelometric Titration)||min. 98.0 %|
|Solubility in water||Soluble|
|Hazard Statements||H314 : Causes severe skin burns and eye damage.
|Precautionary Statements||P260 : Do not breathe dust or mist.
P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection.
P303 + P361 + P353 : IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water.
P301 + P330 + P331 : IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P304 + P340 + P310 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Immediately call a POISON CENTER/doctor.
P305 + P351 + P338 + P310 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER/doctor.
Amino diols (0.5 mmol), K2CO3 (207.3 mg, 1.5 mmol), and p-toluenesulfonyl chloride (190.7 mg, 1.0 mmol) are added to a solution of Cu(OTf)2 (18.1 mg, 0.05 mmol) and (R,R)-2,2'-isopropylidenebis(4-phenyl-2-oxazoline) (16.7 mg, 0.05 mmol) in tert-butyl alcohol (2 mL). After stirring for 12 h at room temperature, water (10 mL) is added. The resulting mixture is extracted with AcOEt. After separation, the organic layer is washed with brine, and then dried over Na2SO4. Concentration and purification through flash column chromatography gives the product.
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