text.skipToContent text.skipToNavigation

Maximum quantity allowed is 999

Please select the quantity

CAS RN: 17564-64-6 | Product Number: A5504

N-Chloromethylphthalimide [for HPLC Labeling]


Purity: >98.0%(T)(HPLC)
Synonyms:
Documents:
5G
¥13,800
9   It can be shipped from Saitama warehouse on the same day* Contact Us
* Please confirm the shipping information for details. If it is displayed as 4 weeks or more, it may be shortened by placing an order.
* For the case that without specific estimated shipping data, e.g.: If displayed as "will be shipped after 8 working days", the products will be shipped 8 working days later after ordering.
* Available Stock: Prompt shipment (for products) in Saitama/Hyogo warehouse. Stock in other WH: 2-3 Business Days
* Please contact us if you need further information.
* To send your quote request for bulk quantities, please click on the "Request Bulk Quote" button. Please note that we cannot offer bulk quantities for some products.
*TCI frequently reviews storage conditions to optimize them. Please note that the latest information on the storage temperature for the products is described on our website.

Product Number A5504
Purity / Analysis Method >98.0%(T)(HPLC)
Grade Ace
Molecular Formula / Molecular Weight C__9H__6ClNO__2 = 195.60 
Physical State (20 deg.C) Solid
Storage Temperature Room Temperature (Recommended in a cool and dark place, <15°C)
CAS RN 17564-64-6
Reaxys Registry Number 140942
PubChem Substance ID 87563154
SDBS (AIST Spectral DB) 23200
MDL Number

MFCD00005898

Specifications
Appearance White to Almost white powder to crystal
Purity(HPLC) min. 98.0 area%
Purity(Argentometric Titration) min. 98.0 %
Melting point 133.0 to 137.0 °C
Solubility in hot Methanol almost transparency
Effect test of HPLC derivatization Effective as labeling agent for Hexanoic Acid , Decanoic Acid , Dodecanoic Acid
Properties (reference)
Melting Point 135 °C
GHS
Pictogram Pictogram
Signal Word Warning
Hazard Statements H315 : Causes skin irritation.
H319 : Causes serious eye irritation.
Precautionary Statements P264 : Wash skin thoroughly after handling.
P280 : Wear protective gloves/ eye protection/ face protection.
P302 + P352 : IF ON SKIN: Wash with plenty of water.
P337 + P313 : If eye irritation persists: Get medical advice/ attention.
P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P362 + P364 : Take off contaminated clothing and wash it before reuse.
P332 + P313 : If skin irritation occurs: Get medical advice/ attention.
Related Laws:
Transport Information:
Application
HPLC Labeling Reagent for Carboxylic Acids

The compound 1 is an HPLC labeling reagent, which has a chloromethyl group and easily reacts with a carboxyl group to form an ester in the presence of a base. The resultant ester is stable and can reach the detector without any decomposition under reversed phase HPLC. An excellent chromatogram can be obtained by measuring at 254 nm, an absorption wavelength that is generally used for UV detection.

Application examples:
[Fatty acids] 1)
Dissolve 3 mg of a sample in 1 mL of acetonitrile, and add 1 mL of the labeling reagent 1 / acetonitrile solution (10 mg / mL) and 1 mL of triethylamine / acetonitrile solution (5 mg / mL). Close the cap of the reaction vessel and incubate the solution at 60 °C for 1 h. Cool the resultant solution to room temperature and use it as an HPLC sample. In the case of using alkali metal salts and crown ethers, the esterification reaction is completed in 5 min at 60 °C. Cool the resultant solution to room temperature and use it as an HPLC sample.

References


PubMed Literature


Articles/Brochures

TCIMAIL
Documents (Note: Some products will not have analytical charts available.)
Safety Data Sheet (SDS)
Please select Language.

The requested SDS is not available.

Please Contact Us for more information.

Specifications
C of A & Other Certificates
Please enter Lot Number Incorrect Lot Number. Please input only the 4-5 alphanumeric characters before the hyphen.

The product with the lot number searched for has been discontinued and no related documentation is available.

Analytical Charts
Please enter Lot Number Incorrect Lot Number. Please input only the 4-5 alphanumeric characters before the hyphen.

The requested analytical chart is not available. Sorry for the inconvenience.

The product with the lot number searched for has been discontinued and no related documentation is available.

Other Documents

Session Status
Your session will timeout in 10 minutes. You will be redirected to the HOME page after session timeout. Please click the button to continue session from the same page. minute. You will be redirected to the HOME page after session timeout. Please click the button to continue session from the same page.

Your session has timed out. You will be redirected to the HOME page.