Published TCIMAIL newest issue No.200
Maximum quantity allowed is 999
Please select the quantity
CAS RN: 952057-61-3 | Product Number: B3234
Benzyl 2,2,2-Trifluoro-N-phenylacetimidate
×
Purity: >98.0%(GC)
Synonyms:
- 2,2,2-Trifluoro-N-phenylacetimidic Acid Benzyl Ester
Product Documents:
| Size | Unit Price | Belgium | Japan* | Quantity |
Shipping Information
|
|---|---|---|---|---|---|
| 1G |
€234.00
|
Contact Us | 9 |
|
|
| 5G |
€750.00
|
1 | 10 |
|
* Stock available in Belgium: Shipment on the same day
* Stock available in Japan: Please check the Shipping Simulation for estimated shipments. (excludes regulated items and dry ice shipments)
| Product Number | B3234 |
Purity / Analysis Method 
|
>98.0%(GC) |
| Molecular Formula / Molecular Weight | C__1__5H__1__2F__3NO = 279.26 |
| Physical State (20 deg.C) | Liquid |
| Storage Temperature
|
Refrigerated (0-10°C) |
| Store Under Inert Gas | Store under inert gas |
| Condition to Avoid | Moisture Sensitive,Heat Sensitive |
| CAS RN | 952057-61-3 |
| Reaxys Registry Number | 11143384 |
| PubChem Substance ID | 87560711 |
Specifications
| Appearance | White or Colorless to Yellow to Green powder to lump to clear liquid |
| Purity(GC) | min. 98.0 % |
Properties (reference)
| Specific Gravity (20/20) | 1.21 |
| Refractive Index | 1.52 |
GHS
| Pictogram |
|
| Signal Word | Warning |
| Hazard Statements | H315 : Causes skin irritation. H319 : Causes serious eye irritation. |
| Precautionary Statements | P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P302 + P352 : IF ON SKIN: Wash with plenty of water. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P362 + P364 : Take off contaminated clothing and wash it before reuse. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. |
Related Laws:
Transport Information:
| HS Number | 2925290090 |
Application
O-Benzylation reaction under non-basic conditions
Typical procedure: To the stirred suspention of B3234 (228.4 mg), ethyl L-mandelate (73.7 mg), MS5A (50 mg) in 1,4-dioxane (4 mL) under N2 atmosphere, TMSOTf (9.1 mg) is added. The reaction mixture is stirred for 1.5 h at 60°C, and then quenched with triethylamine (30 mg). The mixture is filtered to remove MS and evaporated. The resulting residue is purified by preparative TLC (stationary phase: silica-gel, eluant: hexane/diethyl ether) to give the benzylic product in a 91% yield.
References
PubMed Literature
Product Documents (Note: Some products will not have analytical charts available.)
Safety Data Sheet (SDS)
Please select Language.
The requested SDS is not available.
Please Contact Us for more information.
Specifications
C of A & Other Certificates
Please enter Lot Number
Incorrect Lot Number. Please input only the 4-5 alphanumeric characters before the hyphen.
Sample C of A
This is a sample C of A and may not represent a recently manufactured lot of the product.
A sample C of A for this product is not available at this time.
Analytical Charts
Please enter Lot Number
Incorrect Lot Number. Please input only the 4-5 alphanumeric characters before the hyphen.
The requested analytical chart is not available. Sorry for the inconvenience.