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CAS RN: 88-68-6 | Product Number: A0262

2-Aminobenzamide


Purity: >98.0%(T)(HPLC)
Synonyms:
  • Anthranilamide
Documents:
25G
€16.00
4   ≥20 
100G
€32.00
2   5  
500G
€96.00
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Product Number A0262
Purity / Analysis Method >98.0%(T)(HPLC)
Molecular Formula / Molecular Weight C__7H__8N__2O = 136.15  
Physical State (20 deg.C) Solid
CAS RN 88-68-6
Reaxys Registry Number 508509
PubChem Substance ID 87561917
SDBS (AIST Spectral DB) 3326
MDL Number

MFCD00007981

Specifications
Appearance White to Almost white powder to crystal
Purity(HPLC) min. 98.0 area%
Purity(Nonaqueous Titration) min. 98.0 %
Melting point 110.0 to 113.0 °C
Solubility in Methanol almost transparency
Properties (reference)
Melting Point 111 °C
GHS
Pictogram Pictogram
Signal Word Warning
Hazard Statements H315 : Causes skin irritation.
H319 : Causes serious eye irritation.
Precautionary Statements P264 : Wash skin thoroughly after handling.
P280 : Wear protective gloves/ eye protection/ face protection.
P302 + P352 : IF ON SKIN: Wash with plenty of water.
P337 + P313 : If eye irritation persists: Get medical advice/ attention.
P362 + P364 : Take off contaminated clothing and wash it before reuse.
P332 + P313 : If skin irritation occurs: Get medical advice/ attention.
Related Laws:
EC Number 201-851-2
RTECS# CU8993000
Transport Information:
HS Number 2924297086
Application
Synthesis of 4-Hydroxyquinazolines Using Gold’s Reagent

G0393, A0262

A dry, three-necked, round-bottomed flask is equipped with a condenser, thermometer, magnetic stirrer and is placed under a nitrogen atmosphere. Into the flask is placed 100 mL of dry dioxane and 6.8 g (0.05 mol) of 2-aminobenzamide and 9.9 g (0.061 mol) of Gold’s reagent. The resulting mixture is refluxed overnight and subsequently cooled to room temperature. Anhydrous sodium acetate (4.1 g, 0.05 mol) and glacial acetic acid (2 mL) are added and the resulting mixture is refluxed for 3 hr, cooled to room temperature, and the solvent is removed in vacuo. The solid residue is collected by vacuum filtration with the aid of a small amount (15 mL) of water. The solid is vacuum dried to yield 4.9 g (67% yield) of 4-hydroxyquinazoline.

References


PubMed Literature


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