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CAS RN: 1620285-48-4 | Product Number: B4485


Purity: >92.0%(HPLC)
1   5  

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Product Number B4485
Purity / Analysis Method >92.0%(HPLC)
Molecular Formula / Molecular Weight C__6__6H__5__4N__4O__2 = 935.18  
Physical State (20 deg.C) Solid
Storage Temperature <0°C
Store Under Inert Gas Store under inert gas
Condition to Avoid Moisture Sensitive,Heat Sensitive
CAS RN 1620285-48-4
PubChem Substance ID 253660939
Appearance Light yellow to Brown to Dark green powder to crystal
Purity(HPLC) min. 92.0 area%
Elemental analysis(Nitrogen) 5.50 to 6.30 %
Properties (reference)
Related Laws:
Transport Information:
HS Number 2933998090
Asymmetric Iodolactonization Using a Trinuclear Zinc Complex Prepared from Bisaminoiminobinaphthol Ligand


General procedure of the enantioselective iodolactonization: A mixture of 1 (0.001 mmol) and Zn(OAc)2 (0.003 mmol) is stirred for 0.5 hour in anhydrous dichloromethane (1.0 mL) at rt. After cooling the mixture to -78 °C, carboxylic acid (0.1 mmol) in toluene (3.0 mL) is slowly added to the resulting yellow solution and stirred for 0.5 hour at the same temperature. Then, N-iodosuccinimide (NIS) (24.6 mg, 0.11 mmol) and I2 (5.0 mg, 0.02 mmol) are added to the reaction mixture. After being stirred for appropriate time, the reaction mixture is quenched with saturated Na2SO3 aq. and 1N NaOH aq., and then the products are extracted with dichloromethane 3 times. The collected organic layer is dried over Na2SO4. After removal of the solvent under reduced pressure, the residue is purified by silica-gel column chromatography (hexane/acetone=8/1) to afford the iodolactone.


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