CAS RN: 61717-82-6 | Product Number: I0791
2-Iodoxybenzoic Acid (stabilized with Benzoic Acid + Isophthalic Acid)
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|Purity / Analysis Method||>39.0%(T)|
|Molecular Formula / Molecular Weight||C__7H__5IO__4 = 280.02|
|Physical State (20 deg.C)||Solid|
|Store Under Inert Gas||Store under inert gas|
|Condition to Avoid||Light Sensitive,Moisture Sensitive|
|Reaxys Registry Number||976364|
|PubChem Substance ID||172089095|
|Merck Index (14)||5048|
|Appearance||White to Almost white powder to crystal|
|Purity(Iodometric Titration)||39.0 to 50.0 %|
|Melting Point||232 °C(dec.)|
|Hazard Statements||H302 : Harmful if swallowed.
H314 : Causes severe skin burns and eye damage.
H361 : Suspected of damaging fertility or the unborn child.
H372 : Causes damage to organs through prolonged or repeated exposure.
|Precautionary Statements||P260 : Do not breathe dust/ fume/ gas/ mist/ vapours/ spray.
P201 : Obtain special instructions before use.
P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection.
P303 + P361 + P353 : IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water.
P304 + P340 + P310 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Immediately call a POISON CENTER/doctor.
P305 + P351 + P338 + P310 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER/doctor.
Under nitrogen, thioacetal (1.0 mmol) is dissolved in DMSO (5.0 mL) containing a small amount (ca. 0.09 mL) of added H2O and then, IBX (1.5 mmol) is introduced. The mixture is stirred at ambient temperature for 15 min–12 h (depending on the structure of the substrate). When TLC shows completion of the reaction, water (10 mL) is added. The white precipitates are filtered off and washing with ether. The combined filtrate / washings are washed with water and brine, and dried over Na2SO4. The residue after removal of the solvent is chromatographed on silica gel (petroleum ether / ethyl acetate) to give the pure product.
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