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CAS RN: 183266-61-7 | 产品编码: T3174
(Trifluoroacetyl)benzotriazole (mixture of 1H- and 2H- isomers)
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技术规格
| Appearance | White to Almost white powder to crystal |
| Purity(HPLC) | min. 98.0 area% |
| Melting point | 67.0 to 71.0 °C |
| NMR | confirm to structure |
物性（参考值）
| 熔点 | 69 °C |
| 溶解性（可溶于） | 甲醇 |
GHS
| 象形图 |
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| 信号词 | Warning |
| 危险性说明 | H315 : Causes skin irritation. H319 : Causes serious eye irritation. |
| 防范说明 | P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P302 + P352 : IF ON SKIN: Wash with plenty of water. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. P362 + P364 : Take off contaminated clothing and wash it before reuse. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. |
相关法规
运输信息
| HS编码* | 2933.99-000 |
应用
Trifluoroacetylation of Amines
[Experimental procedure]
A solution of 2-phenylethylamine (0.61 g, 5.0 mmol) and (trifluoroacetyl)benzotriazole (1.18 g, 5.5 mmol) in THF (dried, 20 mL) is stirred at room temperature for 4 hours. Then the mixture is diluted with ethyl acetate (20 mL) and washed with aqueous 2 N sodium hydroxide solution (2 x 15 mL). The aqueous layers are extracted with ethyl acetate (20 mL). The combined organic layers are dried over sodium sulfate. After the removal of organic solvent, the crude product is obtained in quantitative yield.
A solution of 2-phenylethylamine (0.61 g, 5.0 mmol) and (trifluoroacetyl)benzotriazole (1.18 g, 5.5 mmol) in THF (dried, 20 mL) is stirred at room temperature for 4 hours. Then the mixture is diluted with ethyl acetate (20 mL) and washed with aqueous 2 N sodium hydroxide solution (2 x 15 mL). The aqueous layers are extracted with ethyl acetate (20 mL). The combined organic layers are dried over sodium sulfate. After the removal of organic solvent, the crude product is obtained in quantitative yield.
References
- (Trifluoroacetyl)benzotriazole: A Convenient Trifluoroacetylating Reagent
PubMed Literature
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