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CAS RN: 35109-88-7 | Product Number: I0759

2-Iodoadenosine


Purity: >98.0%(HPLC)(N)
Synonyms:
  • 6-Amino-2-iodo-9-(β-D-ribofuranosyl)purine
Documents:
200MG
$94.00
5   1  
1G
$340.00
19   7  
5G
$1,087.00
8   1  

* Please contact our distributors or TCI to order our products. The above prices do not include freight cost, customs, and other charges to the destination.
* The storage conditions are subject to change without notice.


Product Number I0759
Purity / Analysis Method >98.0%(HPLC)(N)
Molecular Formula / Molecular Weight C__1__0H__1__2IN__5O__4 = 393.14  
Physical State (20 deg.C) Solid
CAS RN 35109-88-7
Reaxys Registry Number 4546706
PubChem Substance ID 87561674
MDL Number

MFCD01320413

Specifications
Appearance White to Orange to Green powder to crystal
Purity(HPLC) min. 98.0 area%
Purity(with Total Nitrogen) min. 98.0 %
Properties (reference)
Melting Point 144 °C
Maximum Absorption Wavelength 265(H2O) nm
GHS
Related Laws:
Transport Information:
H.S.code* 2940.00-000
*This code is applied to the products when TCI exports from Japan and not for import in your country.
Application
Palladium-catalyzed cross-coupling reaction with terminal alkynes

Typical procedure: 2-Iodoadenosine (393 mg), CuI (9.5 mg), bis(triphenylphosphine)palladium(II) dichloride (36 mg), triethylamine (0.16 mL) and ethynylbenzene (123 mg) in DMF (7 mL) is heated 80 °C for 1 h. After 2-iodoadenosine is completely consumed, the reaction mixture is concentrated to dryness under reduce pressure. The residue is dissolved in CHCl3, and H2S gas is introduced to the solution (~30 s) followed by N2 gas. The suspension is filtered through a Celite pad and washed with CHCl3. The combined filtrate is concentrated to dryness in vacuo, and the residue is purified by a silica gel column chromatography (eluent: MeOH–CHCl3) to give 2-(phenylethyn-1-yl)adenosine (373 mg, 97 %).

References


PubMed Literature


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