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CAS RN: 811-68-7 | Product Number: S0977

Silver(I) Trifluoromethanethiolate


Purity: >95.0%(T)
Synonyms:
  • Trifluoromethanethiol Silver(I) Salt
Documents:
1G
$123.00
≥20  14  
5G
$428.00
≥20  Contact Us

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* The storage conditions are subject to change without notice.


Product Number S0977
Purity / Analysis Method >95.0%(T)
Molecular Formula / Molecular Weight CAgF__3S = 208.93  
Physical State (20 deg.C) Solid
Store Under Inert Gas Store under inert gas
Condition to Avoid Light Sensitive,Air Sensitive
Packaging and Container 1G-Glass Bottle with Plastic Insert (View image)
CAS RN 811-68-7
Reaxys Registry Number 4151922
PubChem Substance ID 354333285
MDL Number

MFCD25563234

Specifications
Appearance White to Light yellow to Light red powder to crystal
Purity(Precipitation Titration) min. 95.0 %
Properties (reference)
Solubility in water Insoluble
Solubility (slightly sol. in) Methanol
GHS
Related Laws:
Transport Information:
H.S.code* 2843.29-000
*This code is applied to the products when TCI exports from Japan and not for import in your country.
Application
Trifluoromethylthiolating Agent Usable for Direct Dehydroxytrifluoromethylthiolation of Alcohols

S0977

Experimental procedure3): AgSCF3 (251 mg, 1.2 mmol, 3.0 eq.) and TBAI (1330 mg, 3.6 mmol, 9.0 eq.) are combined in a Schlenk tube. The tube is mounted with a reflux condenser and backfilled with N2, then toluene (4.0 mL) and alcohol (0.4 mmol, 1.0 eq.) are added. The tube is placed into a preheated oil bath at 80 °C with vigorous stirring. After 10 h, the reaction mixture is cooled to room temperature and filtered through a plug of silica (eluted with EtOAc). The filtrate is concentrated, and the product is purified by column chromatography on silica gel to give the desired product.

References


PubMed Literature


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