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CAS RN: 26042-63-7 | 產品號碼: S0981
Silver Hexafluorophosphate
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| 產品號碼 | S0981 |
純度/分析方法 
|
>98.0%(T) |
| 分子式 / 分子量 | AgPF__6 = 252.83 |
| 外觀與形狀（20°C） | Solid |
| 儲存條件
|
Room Temperature (Recommended in a cool and dark place, <15°C) |
| 儲存在惰性氣體下 | Store under inert gas |
| 應避免的情況 | Light Sensitive,Hygroscopic |
| 包裝和容器
|
1G-Glass Bottle with Plastic Insert （閲覽圖片）, 5G-Glass Bottle with Plastic Insert （閲覽圖片） |
| CAS RN | 26042-63-7 |
| Reaxys-RN | 13607729 |
| PubChem Substance ID | 354333698 |
| MDL編號 | MFCD00003415 |
產品規格
| Appearance | White to Light yellow to Light red powder to crystal |
| Purity(Precipitation Titration) | min. 98.0 % |
| NMR | confirm to structure |
性質
| 熔點 | 102 °C(dec.) |
| Maximum Wavelength | 413 nm (CHCl__3) |
| 水溶性 | Soluble |
GHS
| 圖形表示 |
|
| 信號詞 | Danger |
| 危險性說明 | H314 : Causes severe skin burns and eye damage. H290 : May be corrosive to metals. |
| 防範說明 | P501 : Dispose of contents/ container to an approved waste disposal plant. P260 : Do not breathe dusts or mists. P234 : Keep only in original container. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection. P390 : Absorb spillage to prevent material damage. P303 + P361 + P353 : IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water/shower. P301 + P330 + P331 : IF SWALLOWED: Rinse mouth. Do NOT induce vomiting. P363 : Wash contaminated clothing before reuse. P304 + P340 + P310 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Immediately call a POISON CENTER/doctor. P305 + P351 + P338 + P310 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER/doctor. P406 : Store in corrosive resistant container with a resistant inner liner. P405 : Store locked up. |
相關法規
運輸資料
| UN編號 | UN3260 |
| 類別 | 8 |
| 包裝類別 | II |
| HS編碼* | 2843.29-000 |
Application
A C-Arylation of N-Tosyl Aziridines
Experimental procedure: A mixture of 1 (1 mmol, 273 mg), anisole (2 mmol, 100 µL) and AgPF6 (0.02 mmol, 5 mg) in 3 mL of dry dichloroethane are stirred at 30 - 35 °C. Then the reaction mixture is diluted with water (5 mL) and extracted with dichloroethane (5 mL). The combined organic layers are dried over anhydrous sodium sulfate, concentrated in vacuo and the resulting product is purified by column chromatography on silica gel (ethyl acetate : petroleum ether = 1 : 10) to afford 2 (305 mg, 80% yield).
References
- A facile C-arylation of N-tosyl aziridines via Ag(I) catalysis
PubMed Literature
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