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Chloro(dimethyl)thexylsilane
(CAS RN:67373-56-2 Product Number:T2116)

Structure

Chloro(dimethyl)thexylsilane
Synonym Chlorodimethyl(1,1,2-trimethylpropyl)silane
Synonym Dimethylthexylsilyl Chloride

General Information

Product Number T2116

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Purity/Analysis Method >95.0%(GC)
Storage Temperature
M.F. / M.W. C8H19ClSi=178.78
CAS RN 67373-56-2
Related CAS RN
MDL Number MFCD00012175
Packaging and Container
  • Product Details
  • Safety & Regulations

Specification

Purity(GC) min. 95.0 %
Specific gravity (20/20) 0.9110 to 0.9160
Refractive index n20/D 1.4480 to 1.4520

Data of Reference

flp 46°C(lit.)
bp 56°C/10mmHg(lit.)

References

Reaxys-RN 3647960
PubChem SID 125307411

GHS

Pictogram
Signal Word Danger
Hazard Statements
  • H226
  • :Flammable liquid and vapour.
  • H290
  • :May be corrosive to metals.
  • H314
  • :Causes severe skin burns and eye damage.
Precautionary Statements
  • P260
  • :Do not breathe dusts or mists.
  • P301+P330+P331+P310
  • :IF SWALLOWED: Rinse mouth. Do NOT induce vomiting. Immediately call a POISON CENTER or doctor.
  • P303+P361+P353+P310+P363
  • :IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water or shower. Immediately call a POISON CENTER or doctor. Wash contaminated clothing before reuse.
  • P304+P340+P310
  • :IF INHALED: Remove person to fresh air and keep comfortable for breathing. Immediately call a POISON CENTER or doctor.
  • P305+P351+P338+P310
  • :IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER or doctor.
  • P370+P378
  • :In case of fire: Use dry chemical or dry sand to extinguish.

Transport Information

UN Number 2986
Class 8/3
Packing Group II
HS Number 2931399090

Application

Silylating Agent

Typical Procedure: To chloro(dimethyl)thexylsilane (1.96 g, 11 mmol) and imidazole (1.02 g, 15 mmol) in DMF (5 mL) is added cyclohexanol (1.1 g, 11 mmol) at 25 °C. The mixture is stirred for 16 hrs at ambient temperature and then diluted with hexane. The hexane phase is washed twice with water, dried with MgSO4 and evaporated to furnish, after Kugelrohr distillation, 2.51 g (Y. 94%) of the product, bp 100-105 °C / 0.03 torr.

References

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