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Di(N-succinimidyl) Carbonate
(CAS RN:74124-79-1 Product Number:D1662)

Structure

Di(N-succinimidyl) Carbonate
Synonym N,N'-Disuccinimidyl Carbonate
Synonym DSC
Synonym N-Succinimidyl Carbonate

General Information

Product Number D1662

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Purity/Analysis Method >98.0%(T)
Storage Temperature 0-10°C
M.F. / M.W. C9H8N2O7=256.17
CAS RN 74124-79-1
Related CAS RN
MDL Number MFCD00009767
Packaging and Container
  • Product Details
  • Safety & Regulations

Specification

Appearance White to Gray to Brown powder to crystal
Purity(Butylamine Method) min. 98.0 %
Solubility in hot Pyridine almost transparency

Data of Reference

mp 215°C(dec.)(lit.)

References

Reaxys-RN 1499137
PubChem SID 87568139
F&F 9,208
EC Number 277-730-3

GHS

Pictogram
Signal Word Warning
Hazard Statements
  • H302
  • :Harmful if swallowed.
  • H315
  • :Causes skin irritation.
  • H319
  • :Causes serious eye irritation.
Precautionary Statements
  • P264
  • :Wash hands and face thoroughly after handling.
  • P270
  • :Do not eat, drink or smoke when using this product.
  • P280
  • :Wear protective gloves, eye protection.
  • P301+P312+P330
  • :IF SWALLOWED: Call a POISON CENTER or doctor if you feel unwell. Rinse mouth.
  • P302+P352+P332+P313+P362+P364
  • :IF ON SKIN: Wash with plenty of water. If skin irritation occurs: Get medical advice or attention. Take off contaminated clothing and wash it before reuse.
  • P305+P351+P338+P337+P313
  • :IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. If eye irritation persists: Get medical advice or attention.

Transport Information

HS Number 2925199590

Application

A Condensing Reagent

Experimental procedure3): 1 (10 mg, 0.08 mmol) is dissolved in CH2Cl2 and, to this solution, Et3N (10 mg, 0.1 mmol) and N,N’-disuccinimidyl carbonate (26 mg, 0.1 mmol) are added. The resulting solution is stirred for 30 min after which ethanolamine (6 mg, 0.1 mmol) is added. The reaction is stirred at room temperature for an additional 1 hour. The organic solvent is evaporated and the residue is purified by preparative TLC (EtOAc) to afford 11 mg of compound 2 as a colorless oil, in 81% yield.

References

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