Home >   Products   >  Advanced Search

Allyl Phenyl Carbonate
(CAS RN:16308-68-2 Product Number:A2303)

Structure

Allyl Phenyl Carbonate
Synonym Carbonic Acid Allyl Phenyl Ester

General Information

Product Number A2303

* Items available from stock in Japan will be delivered in 10 business days.
* Please contact us if you need further information.
(Sales Dept Tel: +32 (0)3 735 07 00 E-mail: Sales-EU@TCIchemicals.com)
* To send your quote request for bulk quantities, please click on the “Request Bulk Quotation” button. Please note that for some of our products we cannot offer bulk quantities.
* TCI frequently reviews storage conditions to optimize them. Please note that the latest information on the storage temperature for the products is described on our website.

Purity/Analysis Method >97.0%(GC)
Storage Temperature
M.F. / M.W. C10H10O3=178.19
CAS RN 16308-68-2
Related CAS RN
MDL Number MFCD07784342
Packaging and Container
  • Product Details
  • Safety & Regulations

Specification

Purity(GC) min. 97.0 %
Specific gravity (20/20) 1.1040 to 1.1080
Refractive index n20/D 1.4990 to 1.5030

Data of Reference

bp 78°C/0.2mmHg(lit.)

References

Beilstein 6,158
Reaxys-RN 3253031
PubChem SID 125307508

GHS

Pictogram
Signal Word Warning
Hazard Statements
  • H319
  • :Causes serious eye irritation.
Precautionary Statements
  • P264
  • :Wash hands and face thoroughly after handling.
  • P280
  • :Wear eye protection.
  • P305+P351+P338+P337+P313
  • :IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. If eye irritation persists: Get medical advice or attention.

Transport Information

HS Number 2920901090

Application

Mono Carbamate Protection of Aliphatic Diamines

Typical Procedure (Mono Carbamate Protection of Aliphatic Diamines): Allyl phenyl carbonate (10 mmol) is added to a stirring solution of diamine (5.0 mmol) in absolute EtOH (20 mL). The reaction mixture is stirred over night at room temperature followed by removal of the volatiles in vacuo. H2O (25 mL) is added and the pH adjusted to 3 by addition of aq. HCl (2 M) followed by extraction with CH2Cl2 (2 × 50 mL). The aq phase is then made strongly alkaline by addition of aq. NaOH (2 M) and extracted with CH2Cl2 (3 × 80 mL). The organic phase is dried (Na2SO4), filtered and concentrated in vacuo to afford the desired products.

References

Page Top