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CAS RN: 682-30-4 | Product Number: D3728

Diethyl Vinylphosphonate


Purity: >98.0%(GC)
Synonyms:
  • Vinylphosphonic Acid Diethyl Ester
Documents:
5G
$88.00
1   11   ≥20 

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Product Number D3728
Purity / Analysis Method >98.0%(GC)
Molecular Formula / Molecular Weight C__6H__1__3O__3P = 164.14  
Physical State (20 deg.C) Liquid
Storage Temperature 0-10°C
Condition to Avoid Heat Sensitive
CAS RN 682-30-4
Reaxys Registry Number 507596
PubChem Substance ID 87560563
MDL Number

MFCD00009079

Specifications
Appearance Colorless to Almost colorless clear liquid
Purity(GC) min. 98.0 %
Properties (reference)
Boiling Point 82 °C/15 mmHg
Specific Gravity (20/20) 1.06
Refractive Index 1.43
GHS
Related Laws:
RTECS# TA1150000
Transport Information:
HS Number 2920.90.5100
Application
A Stereoselective synthesis of Z-Enamides

D3728

Experimental procedure1): to a dry flask is charged with amide (0.35 mmol), PdCl2(PhCN)2 (0.017 mmol), and CuCl (0.035 mmol). The reaction vessel is charged with oxygen followed by the addition of chlorobenzene (2 mL) and tetraethyl methylenediphosphonate (TEMDP, 0.035 mmol). The reaction mixture is stirred at 70 °C for 1 min and then diethyl vinylphosphonate (1.05 mmol) is added. The reaction mixture is stirred at 70 °C for 48 h under oxygen atmosphere. After the reaction is over, the solvent is evaporated under reduced pressure and the crude residue is purified by flash column chromatograph.

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