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CAS RN: 617-83-4 | Product Number: D4965
Diethylcyanamide
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Purity: >98.0%(GC)
Synonyms:
Product Documents:
| Size | Unit Price | Belgium | Japan* | Quantity |
|---|---|---|---|---|
| 1G |
€22.00
|
1 | 17 |
|
| 5G |
€104.00
|
1 | ≥40 |
|
*Stock available in Belgium will be delivered in 1 to 3 days
*Stock available in Japan will be delivered in 1 to 2 weeks (excludes regulated items and dry ice shipments).
| Product Number | D4965 |
| Purity / Analysis Method | >98.0%(GC) |
| Molecular Formula / Molecular Weight | C__5H__1__0N__2 = 98.15 |
| Physical State (20 deg.C) | Liquid |
| Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
| CAS RN | 617-83-4 |
| Reaxys Registry Number | 1741595 |
| PubChem Substance ID | 354333557 |
| MDL Number | MFCD00001769 |
Specifications
| Appearance | Colorless to Almost colorless clear liquid |
| Purity(GC) | min. 98.0 % |
Properties (reference)
| Boiling Point | 188 °C |
| Flash point | 69 °C |
| Specific Gravity (20/20) | 0.87 |
| Refractive Index | 1.42 |
GHS
| Pictogram |
|
| Signal Word | Danger |
| Hazard Statements | H301 + H311 + H331 : Toxic if swallowed, in contact with skin or if inhaled. H315 : Causes skin irritation. H319 : Causes serious eye irritation. |
| Precautionary Statements | P261 : Avoid breathing mist or vapours. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection/ hearing protection. P301 + P310 + P330 : IF SWALLOWED: Immediately call a POISON CENTER/doctor. Rinse mouth. P302 + P352 + P312 : IF ON SKIN: Wash with plenty of water. Call a POISON CENTER/doctor if you feel unwell. P403 + P233 : Store in a well-ventilated place. Keep container tightly closed. |
Related Laws:
| EC Number | 210-532-7 |
| RTECS# | GS6300000 |
Transport Information:
| UN Number | UN3276 |
| Class | 6.1 |
| Packing Group | III |
| HS Number | 2926907090 |
Application
Catalytic [2+2+2] Cycloaddition Reaction Using Cyanamides
Experimental procedure: FeI2 (15.6 mg, 0.05 mmol, 10 mol%) and dppp (42.4 mg, 0.1 mmol, 20 mol%) are placed in a dried Schlenk tube. Subsequently, distilled THF (2 mL) is added. The resulting mixture is stirred at room temperature for 30 min to afford an orange-yellow clear solution, at which time Zn dust (6.5 mg, 0.1 mmol, 20 mol%) is added. After an additional 30 min of stirring, 1 (0.5 mmol) is added followed by diethylcyanamide (1 mmol, 2 eq.), and the mixture is stirred for 24 h. The solvent is evaporated, and the crude product is directly purified by silica gel flash column chromatography to give 2 (83% yield) as a colorless oil.
References
- Iron-Catalyzed Cycloaddition Reaction of Diynes and Cyanamides at Room Temperature
PubMed Literature
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