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Published TCIMAIL newest issue No.198
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CAS RN: 13450-90-3 | Product Number: G0359
Gallium(III) Chloride Anhydrous
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Purity: >98.0%
Synonyms:
Product Documents:
| Size | Unit Price | Belgium | Japan* | Quantity |
|---|---|---|---|---|
| 5G |
45,00 €
|
19 | ≥100 |
|
| 25G |
153,00 €
|
2 | ≥100 |
|
*Stock available in Belgium will be delivered in 1 to 3 days
*Stock available in Japan will be delivered in 1 to 2 weeks (excludes regulated items and dry ice shipments).
| Product Number | G0359 |
Purity / Analysis Method 
|
>98.0% |
| Molecular Formula / Molecular Weight | GaCl__3 = 176.07 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature
|
Room Temperature (Recommended in a cool and dark place, <15°C) |
| Store Under Inert Gas | Store under inert gas |
| Condition to Avoid | Moisture Sensitive |
| CAS RN | 13450-90-3 |
| Reaxys Registry Number | 3587236 |
| PubChem Substance ID | 87561610 |
| Merck Index (14) | 4348 |
| MDL Number | MFCD00011018 |
Specifications
| Appearance | White to Almost white powder to crystal |
| Purity | min. 98.0 % |
Properties (reference)
| Melting Point | 78 °C |
| Boiling Point | 201 °C |
| Solubility (soluble in) | Benzene |
GHS
| Pictogram |
|
| Signal Word | Danger |
| Hazard Statements | H314 : Causes severe skin burns and eye damage. H290 : May be corrosive to metals. |
| Precautionary Statements | P260 : Do not breathe dust. P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection/ hearing protection. P303 + P361 + P353 : IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water. P301 + P330 + P331 : IF SWALLOWED: Rinse mouth. Do NOT induce vomiting. P304 + P340 + P310 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Immediately call a POISON CENTER/doctor. P305 + P351 + P338 + P310 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER/doctor. |
Related Laws:
| EC Number | 236-610-0 |
| RTECS# | LW9100000 |
Transport Information:
| UN Number | UN3260 |
| Class | 8 |
| Packing Group | II |
| HS Number | 2827398590 |
Application
Gallium-catalyzed Bromocyanation of Alkynes
Typical Procedure: A flame dried Schlenk flask is charged with GaCl3 (7.0 mg, 0.040 mmol) and ClCH2CH2Cl (1.6 mL), then BrCN (63.6 mg, 0.60 mmol) is added. After stirring at room temperature for 5 min, alkyne (0.40 mmol) is added, and the resulting mixture is stirred at 80 °C. After 12 hrs, the mixture is concentrated in vacuo. The residue is subjected to flash column chromatography on silica gel (hexane : AcOEt = 10 : 1 → 4 : 1) as eluents to afford the corresponding β-bromoacrylonitriles.
References
PubMed Literature
Product Documents (Note: Some products will not have analytical charts available.)
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