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Published TCIMAIL newest issue No.199
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CAS RN: 1809-20-7 | Product Number: P0629
Diisopropyl Phosphite
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Purity: >98.0%(GC)
Synonyms:
- Diisopropyl Phosphonate
- Phosphonic Acid Diisopropyl Ester
- Phosphorous Acid Diisopropyl Ester
Product Documents:
| Size | Unit Price | Belgium | Japan* | Quantity |
|---|---|---|---|---|
| 25G |
€26.00
|
10 | 4 |
|
| 500G |
€234.00
|
1 | 1 |
|
*Stock available in Belgium will be delivered in 1 to 3 days
*Stock available in Japan will be delivered in 1 to 2 weeks (excludes regulated items and dry ice shipments).
| Product Number | P0629 |
Purity / Analysis Method 
|
>98.0%(GC) |
| Molecular Formula / Molecular Weight | C__6H__1__5O__3P = 166.16 |
| Physical State (20 deg.C) | Liquid |
| Storage Temperature
|
Room Temperature (Recommended in a cool and dark place, <15°C) |
| Store Under Inert Gas | Store under inert gas |
| Condition to Avoid | Hygroscopic |
| CAS RN | 1809-20-7 |
| Reaxys Registry Number | 1703675 |
| PubChem Substance ID | 87574790 |
| SDBS (AIST Spectral DB) | 4586 |
| MDL Number | MFCD00117905 |
Specifications
| Appearance | Colorless to Almost colorless clear liquid |
| Purity(GC) | min. 98.0 % |
Properties (reference)
| Boiling Point | 79 °C/14 mmHg |
| Flash point | 112 °C |
| Specific Gravity (20/20) | 1.00 |
| Refractive Index | 1.41 |
| Solubility in water | Soluble |
GHS
| Pictogram |
|
| Signal Word | Warning |
| Hazard Statements | H302 + H332 : Harmful if swallowed or if inhaled. H315 : Causes skin irritation. H319 : Causes serious eye irritation. |
| Precautionary Statements | P501 : Dispose of contents/ container to an approved waste disposal plant. P261 : Avoid breathing mist or vapours. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P304 + P340 + P312 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Call a POISON CENTER/doctor if you feel unwell. |
Related Laws:
| EC Number | 217-317-7 |
| RTECS# | SZ7660000 |
Transport Information:
| HS Number | 2920290090 |
Application
H-Phosphonate-Mediated Amination of Quinoline N-Oxides with Trialkylamines
Typical procedure (R=H, R1=R2=R3=Et): Quinoline-N-oxide (145 mg, 1.0 mmol), triethylamine (304 mg, 3.0 mmol), diisopropyl phosphite (332 mg, 2.0 mmol) and CCl4 (0.5 mL) in THF (15 mL) is stirred at room temperature for 8 h. The solvent is evaporated under vacuum, and the residue is quenched with water (5 mL), extracted with ethyl acetate (3 × 5 mL). The combined organic layers are washed with brine (15 mL) and dried over Na2SO4. After filtration, the solvent is evaporated in vacuo. The crude product is purified by silica gel column chromatography (petroleum ether: ethyl acetate = 10:1) to give N, N-diethylquinolin-2-amine (143 mg, 83%) as a yellow oil.
References
PubMed Literature
Documents
Product Articles
[Research Articles] H-Phosphonate-Mediated Amination of Quinoline N-Oxides with TrialkylaminesProduct Documents (Note: Some products will not have analytical charts available.)
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