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CAS RN: 1668-10-6 | Product Number: G0253

Glycinamide Hydrochloride


Purity: >98.0%(T)
Synonyms:
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Product Number G0253
Purity / Analysis Method >98.0%(T)
Molecular Formula / Molecular Weight C__2H__6N__2O·HCl = 110.54 
Physical State (20 deg.C) Solid
Store Under Inert Gas Store under inert gas
Condition to Avoid Hygroscopic
CAS RN 1668-10-6
Reaxys Registry Number 3554199
PubChem Substance ID 87570430
MDL Number

MFCD00013008

Specifications
Appearance White to Almost white powder to crystal
Purity(Argentometric Titration) min. 98.0 %
Properties (reference)
GHS
Related Laws:
EC Number 216-789-1
Transport Information:
HS Number 2924190090
Application
Application for Peptide Synthesis

Typical Procedure:
To a solution of Boc-ΔTyr(Cl2Bzl)-OH (307 mg, 0.7 mmol), glycinamide hydrochloride (77.4 mg, 0.7 mmol) and Et3N (0.1 mL, 0.7 mmol) in DMF (7 mL) is added EDC·HCl (148 mg. 0.77 mmol) and HOBt (129 mg, 0.84 mmol) at -10°C. The reaction mixture is stirred for 2 h at 0°C. and overnight at room temperature. After the solution is evaporated, the residual is dissolved in EtOAc. The solution is washed with 4% NaHCO3, 10% citric acid and water. The solution is dried and evaporated. The purification is carried out by silica gel column chromatography to give Boc-ΔTyr(Cl2Bzl)-Gly-NH2 (317 mg, 85% yield).
(Δ means dehydro-form.)

References


PubMed Literature


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