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CAS RN: 70-34-8 | Product Number: A5512
2,4-Dinitrofluorobenzene [for HPLC Labeling]
![Chemical Structure of 2,4-Dinitrofluorobenzene [for HPLC Labeling]](/medias/A5512.jpg?context=bWFzdGVyfHJvb3R8NDgzNzR8aW1hZ2UvanBlZ3xhR014TDJobU5DODRPVEU1TnpNNU5qWXlNelkyTDBFMU5URXlMbXB3Wnd8MDNhMWMxMzQ3ZmRiMzJmYmM4ZTNiMTA0MDJkODZkNTE4NWEwMzkyMTk0NTY2OThkNzFiZTg0MjljZTE5YTY3Ng "2,4-Dinitrofluorobenzene [for HPLC Labeling]")
![Thumbnail of 2,4-Dinitrofluorobenzene [for HPLC Labeling]](/medias/A5512.jpg?context=bWFzdGVyfHJvb3R8MTUwNDF8aW1hZ2UvanBlZ3xhRGxrTDJnMVlTODRPVE16TVRneE56VXhNekkyTDBFMU5URXlMbXB3Wnd8ZGJmZjczYTBmYjc4MWZhNmY2NjQ4NTQ3YjRjODBkYTU4N2NmNzJlOThiZDhmNjQ3YzE1YmFiYTc5ZTM2NTNkZQ)
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![2,4-Dinitrofluorobenzene [for HPLC Labeling]](/_ui/responsive/theme-tci/images/missing_product_zoom.webp "2,4-Dinitrofluorobenzene [for HPLC Labeling]")
Purity: >99.0%(GC)
Chemical Substance Law (ENCS):
3-456
Synonyms:
- 1-Fluoro-2,4-dinitrobenzene
Product Documents:
| Size | Unit Price | Saitama (Kawaguchi) | Hyogo (Amagasaki) | Stock in other WH |
Shipping Information
|
|---|---|---|---|---|---|
| 5G |
¥3,600
|
5 | 27 | ≥60 | |
| 25G |
¥11,600
|
≥80 | 23 | It can be shipped in about 2 weeks after ordering |
* Available Stock: Prompt shipment (for products) in Saitama/Hyogo warehouse. Stock In Other WH: Shipment in about 2-3 Business Days from Saitama warehouse. Please contact us
if you need further information.
* The displayed price is the unit price and does not include consumption tax. The unit prices displayed are the latest and are subject to change without notice.
* To send your quote request for bulk quantities, please click on the "Request Bulk Quote" button. Please note that we cannot offer bulk quantities for some products.
*TCI frequently reviews storage conditions to optimize them. Please note that the latest information on the storage temperature for the products is described on our website.
* The displayed price is the unit price and does not include consumption tax. The unit prices displayed are the latest and are subject to change without notice.
* To send your quote request for bulk quantities, please click on the "Request Bulk Quote" button. Please note that we cannot offer bulk quantities for some products.
*TCI frequently reviews storage conditions to optimize them. Please note that the latest information on the storage temperature for the products is described on our website.
| Product Number | A5512 |
Purity / Analysis Method 
|
>99.0%(GC) |
| Grade
|
Ace |
| Molecular Formula / Molecular Weight | C__6H__3FN__2O__4 = 186.10 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature
|
Room Temperature (Recommended in a cool and dark place, <15°C) |
| Store Under Inert Gas | Store under inert gas |
| Condition to Avoid | Air Sensitive |
| CAS RN | 70-34-8 |
| Reaxys Registry Number | 398632 |
| PubChem Substance ID | 87563159 |
| SDBS (AIST Spectral DB) | 10307 |
| Merck Index (14) | 4172 |
| MDL Number | MFCD00007056 |
Specifications
| Appearance | White or Colorless to Yellow to Green powder to lump to clear liquid |
| Purity(GC) | min. 99.0 % |
| Effect test of HPLC derivatization | Effective as labeling agent for Propylamine, Diethylamine |
Properties (reference)
| Melting Point | 26 °C |
| Boiling Point | 296 °C |
| Solubility in water | Insoluble |
| Degree of solubility in water | 400 mg/l 25 °C |
| Solubility (soluble in) | Ether, Ethanol, Benzene |
GHS
| Pictogram |
|
| Signal Word | Danger |
| Hazard Statements | H300 : Fatal if swallowed. H315 : Causes skin irritation. H319 : Causes serious eye irritation. H317 : May cause an allergic skin reaction. |
| Precautionary Statements | P501 : Dispose of contents/ container to an approved waste disposal plant. P261 : Avoid breathing dust/ fume/ gas/ mist/ vapors/ spray. P272 : Contaminated work clothing should not be allowed out of the workplace. P270 : Do not eat, drink or smoke when using this product. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P302 + P352 : IF ON SKIN: Wash with plenty of water. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. P362 + P364 : Take off contaminated clothing and wash it before reuse. P333 + P313 : If skin irritation or rash occurs: Get medical advice/ attention. P301 + P310 + P330 : IF SWALLOWED: Immediately call a POISON CENTER/doctor. Rinse mouth. P405 : Store locked up. |
Related Laws:
| Chemical Substance Law (ENCS) |
3-456 |
| Fire Defense Law | Group-5-II |
| RTECS# | CZ7800000 |
Transport Information:
| UN Number | UN2811 |
| Class | 6.1 |
| Packing Group | II |
Application
HPLC Labeling Reagent for Amines
The compound 1 easily reacts with an amino group to form the corresponding 2,4-dinitrophenylamine derivative. The resultant derivative is stable and can reach the detector without any decomposition under reversed phase HPLC. An excellent chromatogram can be obtained by measuring at 254 nm, an absorption wavelength that is generally used for UV detection.
Application examples:
[Amines]
A sample (free amine) 10 mg, chloroform 1 mL, and labeling regent 1 (10 eq. excess amount of the sample) are mixed, and incubated at 60 °C for 1 h. After cooling to room temperature, use it as an HPLC sample. 1 is also used for derivatization of amino acids.1,2)
[Others]
Aminoglycosides3)
[Amines]
A sample (free amine) 10 mg, chloroform 1 mL, and labeling regent 1 (10 eq. excess amount of the sample) are mixed, and incubated at 60 °C for 1 h. After cooling to room temperature, use it as an HPLC sample. 1 is also used for derivatization of amino acids.1,2)
[Others]
Aminoglycosides3)
TCI Products Pamphlet
HPLC Labeling Reagents ( PDF 10MB )
HPLC Labeling Reagents ( PDF 10MB )
References
- 1)Y. Suzuki, Program and Abstracts 6th Congress of Liquid Chromatography (October 1985), 71.
- 2)S. A. Cockle, H. Kaplan, M. A. Hefford, N. M. Young, 1st High-Perform. Liq. Chromatogr. Proteins Pept., Proc. Int. Symp. 1983, 103.
- 3)D. M. Barends, J. S. Blauw, C. W. Mijnsbergen, C. J. L. R. Govers, A. Hulshoff, J. Chromatogr. 1985, 322, 321.
PubMed Literature
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Other Documents
Related Products
2,4-Dinitrofluorobenzene
| Product # | D0835 |
| CAS RN | 70-34-8 |
| Purity / Analysis Method: | >99.0%(GC) |