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CAS RN: 893413-42-8 | Product Number: C3461
(6-Chloro-1H-benzotriazol-1-yloxy)tripyrrolidinophosphonium Hexafluorophosphate
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Purity: >98.0%(HPLC)
Synonyms:
- TPTDP
Product Documents:
| Size | Unit Price | Saitama (Kawaguchi) | Hyogo (Amagasaki) | Stock in other WH |
Shipping Information
|
|---|---|---|---|---|---|
| 5G |
¥1,900
|
6 | 14 | 2 |
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* The displayed price is the unit price and does not include consumption tax. The unit prices displayed are the latest and are subject to change without notice.
* To send your quote request for bulk quantities, please click on the "Request Bulk Quote" button. Please note that we cannot offer bulk quantities for some products.
*TCI frequently reviews storage conditions to optimize them. Please note that the latest information on the storage temperature for the products is described on our website.
| Product Number | C3461 |
| Purity / Analysis Method | >98.0%(HPLC) |
| Molecular Formula / Molecular Weight | C__1__8H__2__7ClF__6N__6OP__2 = 554.84 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature | Refrigerated (0-10°C) |
| Store Under Inert Gas | Store under inert gas |
| Condition to Avoid | Moisture Sensitive,Heat Sensitive |
| CAS RN | 893413-42-8 |
| Reaxys Registry Number | 12838887 |
| PubChem Substance ID | 354335200 |
| MDL Number | MFCD14560589 |
Specifications
| Appearance | White to Light yellow powder to crystal |
| Purity(HPLC) | min. 98.0 area% |
| NMR | confirm to structure |
Properties (reference)
| Melting Point | 173 °C(dec.) |
GHS
| Pictogram |
|
| Signal Word | Warning |
| Hazard Statements | H315 : Causes skin irritation. H319 : Causes serious eye irritation. |
| Precautionary Statements | P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P302 + P352 : IF ON SKIN: Wash with plenty of water. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. P362 + P364 : Take off contaminated clothing and wash it before reuse. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. |
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Application
Condensing Agent
Experimental procedure:
1 (0.5 g, 2.75 mmol) is dissolved in CH2Cl2 (5 mL). 2 (2.2 g, 5.5 mmol), DIEA (1.9 mL, 1.1 mmol), and TPTDP (3.057 g, 5.5 mmol) are dissolved in CH2Cl2 (5 mL). After 2 is dissolved, it is added to the solution of 1 and stirred overnight. The mixture is concentrated under reduced pressure. The methyl ester is removed using 1 mol/L LiOH (30 mL)/MeOH (70 mL) for 4 h. The mixture is acidified by the addition of 3 mol/L HCl (30 mL). MeOH is then removed by evaporation. Ethyl acetate (50 mL) and saturated NaCl (100 mL) is added, followed by extraction 4 times with ethyl acetate (50mL). The organic fractions are combined and the ethyl acetate is concentrated under reduced pressure. The crude is purified by RP-HPLC (CH3CN:H2O:TFA) to give 3 as a white solid.
1 (0.5 g, 2.75 mmol) is dissolved in CH2Cl2 (5 mL). 2 (2.2 g, 5.5 mmol), DIEA (1.9 mL, 1.1 mmol), and TPTDP (3.057 g, 5.5 mmol) are dissolved in CH2Cl2 (5 mL). After 2 is dissolved, it is added to the solution of 1 and stirred overnight. The mixture is concentrated under reduced pressure. The methyl ester is removed using 1 mol/L LiOH (30 mL)/MeOH (70 mL) for 4 h. The mixture is acidified by the addition of 3 mol/L HCl (30 mL). MeOH is then removed by evaporation. Ethyl acetate (50 mL) and saturated NaCl (100 mL) is added, followed by extraction 4 times with ethyl acetate (50mL). The organic fractions are combined and the ethyl acetate is concentrated under reduced pressure. The crude is purified by RP-HPLC (CH3CN:H2O:TFA) to give 3 as a white solid.
References
- Small Molecule Mimetics of an HIV-1 gp41 Fusion Intermediate as Vaccine Leads
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