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CAS RN: 1420299-84-8 | Product Number: C3328

Chloro[(1,2,3,4,5,6-η)-2,2'',4,4'',6,6''-hexamethyl[1,1':3',1''-terphenyl]-2'-thiolato-κS][tris(4-fluorophenyl)phosphine-κP]ruthenium(II)


Purity:
Synonyms:
  • [(DmpSR')RuCl(P-(4-Fluorophenyl)3)]
Documents:
100MG
₹13,800
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Product Number C3328
Molecular Formula / Molecular Weight C__4__2H__3__7ClF__3PRuS = 798.31  
Physical State (20 deg.C) Solid
CAS RN 1420299-84-8
Reaxys Registry Number 23375447
PubChem Substance ID 354334201
Specifications
Appearance Light yellow to Amber to Dark green powder to crystal
Elemental analysis(Carbon) 60.50 to 65.50 %
Elemental analysis(Hydrogen) 4.40 to 5.00 %
Properties (reference)
GHS
Related Laws:
Transport Information:
Application
Hydrodefluorination of Trifluoromethyl Group Using a Ruthenium Catalyst

Experimental procedure: A reaction tube is charged in a glovebox with a mixture of 1 (3.6 mg, 2.3 µmol) and CH3ONa (1.2 µmol). After addition of tetracosane (2.0 mg) as internal standard, n-hexane (0.5 mL) and diphenylmethylsilane (20 mg, 0.10 mmol) are added dropwise to the suspension. N,N-Diethyl-3-trifluoromethylaniline (5.0 mg, 23 µmol) is added, and the reaction mixture is maintained at ambient temperature for 6 h. Product formation is monitored by GLC and verified by GLC-MS.

References


PubMed Literature


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