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Product Document Searching Made Easy by 2D Code! | [Product Highlights] Endogenous Biotin-Blocking Reagent...Maximum quantity allowed is 999
CAS RN: 719-98-2 | Product Number: T3143
N-(Trifluoromethylthio)phthalimide

Purity: >98.0%(GC)
Size | Unit Price | Hyderabad | Japan* | Quantity |
---|---|---|---|---|
1G |
₹10,200.00
|
2 | 7 |
|
5G |
₹44,300.00
|
Contact Us | 17 |
|
*Upon orders receipt, Hyderabad stocks will be dispatched on the same day.
*Items available in Japan warehouse will be dispatched in 10-12 working days.
*INR price is exclusive of domestic taxes applicable.
*TCI frequently reviews storage conditions to optimize them. Please note that the latest information on the storage temperature for the products is described on our website.
Product Number | T3143 |
Purity / Analysis Method | >98.0%(GC) |
Molecular Formula / Molecular Weight | C__9H__4F__3NO__2S = 247.19 |
Physical State (20 deg.C) | Solid |
Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
Store Under Inert Gas | Store under inert gas |
Condition to Avoid | Air Sensitive |
Packaging and Container | 1G-Glass Bottle with Plastic Insert (View image) |
CAS RN | 719-98-2 |
Reaxys Registry Number | 1464619 |
PubChem Substance ID | 253662481 |
Appearance | White to Almost white powder to crystal |
Purity(GC) | min. 98.0 % |
Melting point | 111.0 to 115.0 °C |
Melting Point | 113 °C |
Pictogram |
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Signal Word | Warning |
Hazard Statements | H315 : Causes skin irritation. H319 : Causes serious eye irritation. |
Precautionary Statements | P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P302 + P352 : IF ON SKIN: Wash with plenty of water. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. P362 + P364 : Take off contaminated clothing and wash it before reuse. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. |
CuCl (4.0 mg, 0.04 mmol, 10 mol%), dry boronic acid (0.4 mmol, 1.0 eq.), dry K2CO3 (111 mg, 0.8 mmol, 2.0 eq.), 2,2’-bipyridine (12.5 mg, 0.08 mmol, 20 mol%) and N-(trifluoromethylthio)phthalimide (103.8 mg, 0.42 mmol, 1.05 eq.) are placed into an oven-dried Schlenk tube equipped with a stirring bar. The tube is sealed with a rubber stopper, evacuated and back-filled with dry argon (three times). Dry, freshly distilled and degassed DME is added by a syringe and the reaction mixture is stirred at 45 °C for 18 h. The reaction mixture is cooled to room temperature, diluted with diethyl ether (5 mL), and filtered through a short plug of silica, eluting with additional diethyl ether (50 mL). The filtrate is concentrated; pentane (10 mL) is added and concentrated again for removing residual DME. The resulting residue is purified by chromatography (pentane―diethyl ether) to provide the desired product.
References
- 1)Trifluoromethylsulfenylation of masked carbonyl compounds
- 2)N-Trifluoromethylthiophthalimide: a stable electrophilic SCF3-reagent and its application in the catalytic asymmetric trifluoromethylsulfenylation
- 3)Direct catalytic trifluoromethylthiolation of boronic acids and alkynes employing electrophilic shelf-stable N-(trifluoromethylthio)phthalimide
Documents
Safety Data Sheet (SDS)
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Specifications
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