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Alkylation Reagents for Ester Synthesis
No.168(January 2016)
O-Alkylisoureas (1) to (5) are convenient and useful esterification reagents for the direct alkylation of carboxylic acids. For example, Golding et al. have reported the esterification of 1-cyclobutenecarboxylic acid using 1, affording the corresponding methyl ester.1)
Moreover, Linclau et al. have reported the microwave-accelerated esterification of carboxylic acids using 4 and 5, affording the corresponding esters in excellent yields within several minutes.2)
For another example, the esterification reaction using 2 and 3 also has been reported as below.3)
References
- 1)Resistance-modifying agents. 8. Inhibition of O6-alkylguanine-DNA alkyltransferase by O6-alkenyl-, O6-cycloalkenyl-, and O6-(2-oxoalkyl)guanines and potentiation of temozolomide cytotoxicity in vitro by O6-(1-cyclopentenylmethyl)guanine
- 2)Microwave-accelerated O-alkylation of carboxylic acids with O-alkylisoureas
- 3)Kinetic resolution of racemic α-tert-alkyl-α-hydroxy esters by enantiomer-selective carbamoylation
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