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CAS RN: 35109-88-7 | Product Number: I0759
2-Iodoadenosine
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Purity: >98.0%(HPLC)(N)
Synonyms:
- 6-Amino-2-iodo-9-(β-D-ribofuranosyl)purine
Product Documents:
| Size | Unit Price | Same Day | 2-3 Business Days | Other Lead Time |
Shipping Information
|
|---|---|---|---|---|---|
| 200MG |
₩177,500
|
4 | 1 | It can be shipped in about 2 weeks after ordering | |
| 1G |
₩643,500
|
10 | 5 | It can be shipped in about 2 weeks after ordering | |
| 5G |
₩2,063,100
|
3 | 0 | It can be shipped in about 2 weeks after ordering |
* Please contact our distributor of SEJIN CI Co., Ltd.
if you would like to purchase TCI products. The above prices do not include freight cost, customs charge and other charges to the destination. SEJIN CI Co., Ltd. (Phone: 02-2655-2480 / email:
sales@sejinci.co.kr)
* The storage conditions are subject to change without notice.
* The storage conditions are subject to change without notice.
| Product Number | I0759 |
Purity / Analysis Method 
|
>98.0%(HPLC)(N) |
| Molecular Formula / Molecular Weight | C__1__0H__1__2IN__5O__4 = 393.14 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature
|
Room Temperature (Recommended in a cool and dark place, <15°C) |
| Packaging and Container
|
1G-Glass Bottle with Plastic Insert (View image) |
| CAS RN | 35109-88-7 |
| Reaxys Registry Number | 4546706 |
| PubChem Substance ID | 87561674 |
| MDL Number | MFCD01320413 |
Specifications
| Appearance | White to Orange to Green powder to crystal |
| Purity(HPLC) | min. 98.0 area% |
| Purity(with Total Nitrogen) | min. 98.0 % |
| NMR | confirm to structure |
Properties (reference)
| Melting Point | 144 °C |
| Maximum Absorption Wavelength | 265 nm (H__2O) |
GHS
Related Laws:
Transport Information:
| H.S.code* | 2940.00-000 |
Application
Palladium-catalyzed cross-coupling reaction with terminal alkynes
Typical procedure: 2-Iodoadenosine (393 mg), CuI (9.5 mg), bis(triphenylphosphine)palladium(II) dichloride (36 mg), triethylamine (0.16 mL) and ethynylbenzene (123 mg) in DMF (7 mL) is heated 80 °C for 1 h. After 2-iodoadenosine is completely consumed, the reaction mixture is concentrated to dryness under reduce pressure. The residue is dissolved in CHCl3, and H2S gas is introduced to the solution (~30 s) followed by N2 gas. The suspension is filtered through a Celite pad and washed with CHCl3. The combined filtrate is concentrated to dryness in vacuo, and the residue is purified by a silica gel column chromatography (eluent: MeOH–CHCl3) to give 2-(phenylethyn-1-yl)adenosine (373 mg, 97 %).
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