CAS RN: 64443-05-6 | Product Number: T2665
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|Purity / Analysis Method||>97.0%(T)|
|Molecular Formula / Molecular Weight||C__8H__1__2CuF__6N__4P = 372.72|
|Physical State (20 deg.C)||Solid|
|Store Under Inert Gas||Store under inert gas|
|Condition to Avoid||Air Sensitive,Moisture Sensitive,Heat Sensitive|
|Reaxys Registry Number||14262634|
|PubChem Substance ID||87561580|
|Appearance||White to Almost white powder to crystal|
|Purity(Potassium permanganate method)||min. 97.0 %|
|Melting Point||160 °C(dec.)|
|Hazard Statements||H315 : Causes skin irritation.
H319 : Causes serious eye irritation.
|Precautionary Statements||P264 : Wash skin thoroughly after handling.
P280 : Wear protective gloves/ eye protection/ face protection.
P302 + P352 : IF ON SKIN: Wash with plenty of water.
P337 + P313 : If eye irritation persists: Get medical advice/ attention.
P362 + P364 : Take off contaminated clothing and wash it before reuse.
P332 + P313 : If skin irritation occurs: Get medical advice/ attention.
- Perfluoroalkylation of Unactivated Alkenes with Acid Anhydrides as the Perfluoroalkyl Source
- Catalytic Asymmetric Synthesis of Chiral Tertiary Organoboronic Esters through Conjugate Boration of β-Substituted Cyclic Enones
- Searching for Practically Useful P-Chirogenic Phosphine Ligands
To a stirred mixture of [Cu(CH3CN)4]PF6 (0.010 g, 0.026 mmol) and neocuproine (0.005 g, 0.024 mmol) in the arene (ca. 1 mL) is added N-tosyloxy-2,2,2-trichloroethylcarbamate (0.050 g, 0.138 mmol) and the mixture is allowed to stir at 140 °C for 8 h. The reaction mixture is cooled to room temperature, filtered through a pad of silica, washed with CH2Cl2, and the filtrate is concentrated under vacuum. The residue is purified by silica chromatography using 5–15% Et2O in hexanes to obtain the regioisomeric mixture of aminated arenes. The isomer ratio is determined by NMR using 1,3,5-trimethoxybenzene as a reference.
[Research Articles] Catalytic Asymmetric Vinylogous Conjugate Addition of Unsaturated Butyrolactones to α,β-Unsaturated Thioamides
[Research Articles] Copper-catalyzed C—H Amidation of Unactivated Arenes
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