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CAS RN: 86340-94-5 | Product Number: I0784
N-Iodosaccharin
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Purity: >98.0%(T)
Synonyms:
- 2-Iodo-1,2-benzisothiazol-3(2H)-one 1,1-Dioxide
Product Documents:
| Size | Unit Price | Philadelphia, PA | Portland, OR | Japan* | Quantity |
Shipping Information
|
|---|---|---|---|---|---|---|
| 5G |
$389.00
|
1 | 1 | 11 |
|
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| Product Number | I0784 |
Purity / Analysis Method 
|
>98.0%(T) |
| Molecular Formula / Molecular Weight | C__7H__4INO__3S = 309.08 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature
|
Refrigerated (0-10°C) |
| Store Under Inert Gas | Store under inert gas |
| Condition to Avoid | Light Sensitive,Moisture Sensitive,Heat Sensitive |
| CAS RN | 86340-94-5 |
| Reaxys Registry Number | 177561 |
| PubChem Substance ID | 125307654 |
| MDL Number | MFCD09037939 |
Specifications
| Appearance | White to Light yellow to Light orange powder to crystal |
| Purity(Iodometric Titration) | min. 98.0 % |
Properties (reference)
GHS
| Pictogram |
|
| Signal Word | Warning |
| Hazard Statements | H315 : Causes skin irritation. H319 : Causes serious eye irritation. |
| Precautionary Statements | P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. P302 + P352 : IF ON SKIN: Wash with plenty of soap and water. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. P362 : Take off contaminated clothing and wash before reuse. |
Related Laws:
Transport Information:
| HS Number | 2934.10.2000 |
Application
N-Halosaccharin Usable for Halogenations
Experimental procedure: 1 (142 mg, 0.5 mmol) and LiClO4 (32 mg, 0.3 mmol) are dissolved in CH3CN (10 mL). The reaction mixture is stirred at room temperature for 15 min. N-Iodosaccharin (0.55 mmol) is added and stirring is continued for an additional 30 min. After removal of the solvent, the residue is dissolved in CH2Cl2 (10 mL), washed with strd. aq. NaHCO3 (3 x 10 mL), dried over Na2SO4, filtered and the solvent is evaporated in vacuo. The solid is suspended in CH3OH (4 mL) and, to remove the unwanted saccharin, undissolved pure product is filtered to obtain 2 (188 mg, 92% yield) as a white solid.
References
- Highly regioselective halogenation of 1-phenyl-3-(3,5-dimethoxyphenyl)-propane-1,3-dione
Application
Electrophilic Iodinating Reagent
Reference
PubMed Literature
Documents
Product Articles
[TCIMAIL No.150] Electrophilic Iodinating Reagent[Product Highlights] N-Halosaccharins Usable for Halogenations
[Product Highlights] Electrophilic Iodinating Reagent
Product Documents (Note: Some products will not have analytical charts available.)
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Specifications
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