text.skipToContent text.skipToNavigation

Maximum quantity allowed is 999

Please select the quantity

CAS RN: 830-74-0 | Product Number: A2943

1-Allylisatin


Purity: >98.0%(GC)
Synonyms:
  • 1-Allylindole-2,3-dione
  • 1-Allyl-2,3-indolinedione
Documents:
1G
$175.00
1   1   30  

* Items in stock locally ship in 1-2 business days. Items from Japan stock are able to ship from a US warehouse within 2 weeks. Please contact TCI for lead times on items not in stock. Excludes regulated items and items that ship on ice.
* To send your quote request for bulk quantities, please click on the "Request Quote" button. Please note that we cannot offer bulk quantities for some products.
*TCI frequently reviews storage conditions to optimize them. Please note that the latest information on the storage temperature for the products is described on our website.


Product Number A2943
Purity / Analysis Method >98.0%(GC)
Molecular Formula / Molecular Weight C__1__1H__9NO__2 = 187.20 
Physical State (20 deg.C) Solid
CAS RN 830-74-0
Reaxys Registry Number 1528099
PubChem Substance ID 354333758
MDL Number

MFCD00224218

Specifications
Appearance White to Light yellow to Red powder to crystal
Purity(GC) min. 98.0 %
Melting point 84.0 to 88.0 °C
Properties (reference)
Melting Point 86 °C
Boiling Point 145 °C/1 mmHg
Maximum Absorption Wavelength 267 nm
GHS
Pictogram Pictogram
Signal Word Warning
Hazard Statements H315 : Causes skin irritation.
H319 : Causes serious eye irritation.
Precautionary Statements P264 : Wash skin thoroughly after handling.
P280 : Wear protective gloves/ eye protection/ face protection.
P337 + P313 : If eye irritation persists: Get medical advice/ attention.
P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P302 + P352 : IF ON SKIN: Wash with plenty of soap and water.
P332 + P313 : If skin irritation occurs: Get medical advice/ attention.
P362 : Take off contaminated clothing and wash before reuse.
Related Laws:
Transport Information:
HS Number 2933.99.7900
Application
Multicomponent Reactions involving Arynes, Heterocycles, and Isatins

Experimental procedure: To a screw-capped test tube equipped is added 18-crown 6-ether (0.396 g, 1.5 mmol), KF (0.087 g, 1.5 mmol) and 1 (0.094 g, 0.50 mmol). Then the tube is evacuated and backfilled with argon. The mixture is dissolved in THF (2.0 mL). The resultant reaction mixture is kept stirring at 30 °C for 5 min. To the stirring solution is added pyridine (0.060 g, 0.75 mmol) and the 2-(trimethylsilyl)phenyl trifluoromethane sulfonate (0.223 g, 0.75 mmol) and the reaction mixture is stirred for 12 h at 30 °C. The reaction stops and the crude reaction mixture is purified by column chromatography (Pet. ether:EtOAc = 75 : 25) on silica gel to afford 2 (0.126 g, 73%) as a yellow solid.

References


PubMed Literature


Documents (Note: Some products will not have analytical charts available.)
Safety Data Sheet (SDS)
Please select Language.

The requested SDS is not available.

Please Contact Us for more information.

Specifications
C of A & Other Certificates
Please enter Lot Number Incorrect Lot Number. Please input only the 4-5 alphanumeric characters before the hyphen.
Analytical Charts
Please enter Lot Number Incorrect Lot Number. Please input only the 4-5 alphanumeric characters before the hyphen.

The requested analytical chart is not available. Sorry for the inconvenience.

Other Documents

Session Status
Your session will timeout in 10 minutes. You will be redirected to the HOME page after session timeout. Please click the button to continue session from the same page. minute. You will be redirected to the HOME page after session timeout. Please click the button to continue session from the same page.

Your session has timed out. You will be redirected to the HOME page.