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CAS RN: 86393-33-1 | Product Number: C2293
7-Chloro-1-cyclopropyl-6-fluoro-1,4-dihydro-4-oxoquinoline-3-carboxylic Acid
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Purity: >98.0%(T)(HPLC)
Synonyms:
- Fluoroquinolonic Acid
Documents:
| Size | Unit Price | Philadelphia, PA | Portland, OR | Japan* | Quantity |
|---|---|---|---|---|---|
| 5G |
$39.00
|
2 | 1 | 31 |
|
| 25G |
$102.00
|
1 | 1 | 14 |
|
* Items in stock locally ship in 1-2 business days. Items from Japan stock are able to ship from a US warehouse within 2 weeks. Please contact TCI for lead times on items not in stock. Excludes regulated items and items that ship on ice.
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Specifications
| Appearance | White to Light yellow powder to crystal |
| Purity(HPLC) | min. 98.0 area% |
| Purity(Neutralization titration) | min. 98.0 % |
Properties (reference)
| Melting Point | 244 °C |
GHS
| Pictogram |
|
| Signal Word | Danger |
| Hazard Statements | H310 : Fatal in contact with skin. H302 : Harmful if swallowed. H412 : Harmful to aquatic life with long lasting effects. |
| Precautionary Statements | P501 : Dispose of contents/ container to an approved waste disposal plant. P273 : Avoid release to the environment. P270 : Do not eat, drink or smoke when using this product. P262 : Do not get in eyes, on skin, or on clothing. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ protective clothing. P362 : Take off contaminated clothing and wash before reuse. P301 + P312 + P330 : IF SWALLOWED: Call a POISON CENTER/doctor if you feel unwell. Rinse mouth. P302 + P350 + P310 : IF ON SKIN: Gently wash with plenty of soap and water. Immediately call a POISON CENTER or doctor/ physician. P405 : Store locked up. |
Related Laws:
| RTECS# | VB1993795 |
Transport Information:
| HS Number | 2933.49.7000 |
Application
Amination with morpholine derivatives under microwave irradiation
Reference
Application
Synthesis and metabolic evaluation of azaspirocyclic fluoroquinolones
Typical procedure: KOtBu (191 mg) is dissolve in DMSO (20 mL), azetidinium oxalate (164 mg) is added and the mixture is stirred at rt for 10 min. Then, 7-chloro-1-cyclopropyl-6-fluoro-1,4-dihydro-4-oxoquinoline-3-carboxylic acid (200 mg) is added, and the yellow mixture is heated to 130 °C and stirred for 5.5 h. Then it is cooled to rt and poured into H2O (75 mL). The precipitate is filtered and dried overnight upon standing. The crude product is purified by suspending in hot CHCl3, and cooling the mixture to rt, when it is filtered. The residue is dried in vacuo to give the pure desired product (166 mg, 68 %).
References
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