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CAS RN: 7550-35-8 | Product Number: L0210

Lithium Bromide


Purity: >99.0%(T)
Synonyms:
Documents:
25G
$55.00
5   1   ≥100 
100G
$98.00
4   1   ≥60 
500G
$181.00
13   2   ≥40 

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Product Number L0210
Purity / Analysis Method >99.0%(T)
Molecular Formula / Molecular Weight LiBr = 86.84 
Physical State (20 deg.C) Solid
Storage Temperature Room Temperature (Recommended in a cool and dark place, <15°C)
CAS RN 7550-35-8
PubChem Substance ID 87561397
Merck Index (14) 5526
MDL Number

MFCD00011077

Specifications
Appearance White powder to crystal
Purity(Argentometric Titration) min. 99.0 %
Properties (reference)
Melting Point 549 °C
Solubility (soluble in) Acetone
GHS
Pictogram Pictogram
Signal Word Warning
Hazard Statements H302 : Harmful if swallowed.
H315 : Causes skin irritation.
H319 : Causes serious eye irritation.
H402 : Harmful to aquatic life.
Precautionary Statements P501 : Dispose of contents/ container to an approved waste disposal plant.
P273 : Avoid release to the environment.
P270 : Do not eat, drink or smoke when using this product.
P264 : Wash skin thoroughly after handling.
P280 : Wear protective gloves/ eye protection/ face protection.
P337 + P313 : If eye irritation persists: Get medical advice/ attention.
P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P302 + P352 : IF ON SKIN: Wash with plenty of soap and water.
P332 + P313 : If skin irritation occurs: Get medical advice/ attention.
P362 : Take off contaminated clothing and wash before reuse.
P301 + P312 + P330 : IF SWALLOWED: Call a POISON CENTER/doctor if you feel unwell. Rinse mouth.
Related Laws:
RTECS# OJ5755000
Transport Information:
HS Number 2827.59.5100
Application
Sodium- and Ammonia-Free Birch Reduction by Electroreduction

Experimental procedure: An electrochemical cell with magnesium as the anode and galvanized steel wire as the cathode is added to a substrate (0.1 mmol, 1.0 eq.), 1,3-dimethylurea (0.3 mmol, 3.0 eq), tripyrrolidinophosphine oxide (1.0 mmol, 10 eq.), and 1.5 mol/L THF solution of LiBr (500 µL). The reaction mixture is added to THF (3 mL) and is purged with argon. Electrolysis is initiated at a cell ampere of 10 mA at room temperature. After full consumption of substrate, the cell is washed with diethyl ether, and solvent is removed in vacuo. To residue solution is added diethyl ether and solution of Rochelle salt, and then is stirred until two clear layers formed. The organic layer is separated, and the aqueous layer is extracted twice with diethyl ether. The combined organic layers are dried over anhydrous MgSO4. After the organics removed in vacuo, the residue is purified by short silica colum (elution: ethyl acetate) to give product.

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