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CAS RN: 994-30-9 | Product Number: T0589
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|Purity / Analysis Method||>97.0%(GC)|
|Molecular Formula / Molecular Weight||C__6H__1__5ClSi = 150.72|
|Physical State (20 deg.C)||Liquid|
|Store Under Inert Gas||Store under inert gas|
|Condition to Avoid||Moisture Sensitive|
|Reaxys Registry Number||1732860|
|PubChem Substance ID||87576486|
|SDBS (AIST Spectral DB)||5610|
|Appearance||Colorless to Light yellow clear liquid|
|Purity(GC)||min. 97.0 %|
|Boiling Point||149 °C|
|Flash point||30 °C|
|Specific Gravity (20/20)||0.90|
|Hazard Statements||H314 : Causes severe skin burns and eye damage.
H226 : Flammable liquid and vapor.
H290 : May be corrosive to metals.
|Precautionary Statements||P501 : Dispose of contents/ container to an approved waste disposal plant.
P240 : Ground/bond container and receiving equipment.
P210 : Keep away from heat/sparks/open flames/hot surfaces. No smoking.
P233 : Keep container tightly closed.
P234 : Keep only in original container.
P243 : Take precautionary measures against static discharge.
P241 : Use explosion-proof electrical/ ventilating/ lighting/ equipment.
P242 : Use only non-sparking tools.
P264 : Wash skin thoroughly after handling.
P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection.
P370 + P378 : In case of fire: Use dry sand, dry chemical or alcohol-resistant foam to extinguish.
P390 : Absorb spillage to prevent material damage.
P303 + P361 + P353 : IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water/shower.
P301 + P330 + P331 : IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P363 : Wash contaminated clothing before reuse.
P304 + P340 + P310 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Immediately call a POISON CENTER/doctor.
P305 + P351 + P338 + P310 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER/doctor.
P403 + P235 : Store in a well-ventilated place. Keep cool.
P406 : Store in corrosive resistant container with a resistant inner liner.
P405 : Store locked up.
|UN Number (DOT-AIR)||UN2986|
|Packing Group (TCI-A)||II|
To a solution of (±)-1-phenylethyl alcohol (0.242 mL, 2.0 mmol) in THF (4 mL, 0.5 mol/L) was added imidazole (204 mg, 3.0 mmol), then TESCl (0.402 mL, 2.4 mmol) was added dropwise and the mixture was stirred at room temperature for 2 hours. Water (10 mL), ethyl acetate (20 mL) was added to the reaction mixture to quench and was extracted with ethyl acetate (10 mL x 3). The combined organic layer was dried over sodium sulfate and filtered. The solvent was removed under reduced pressure and the residue was purified by column chromatography (ethyl acetate:hexane = 0:100 - 3:97 on silica gel) to give triethyl((±)-1-phenylethoxy)silane as a colorless liquid (373 mg, 79%).
The reaction mixture was monitored by TLC (ethyl acetate:hexane = 1:20, Rf = 0.70).
1H NMR (270 MHz, CDCl3); δ 7.36-7.18 (m, 5H), 4.86 (q, 1H, J = 6.2 Hz), 1.42 (d, 1H, J = 6.2 Hz), 0.94-0.87 (m, 9H), 0.64-0.51 (m, 6H).
- Synthetic Versatility of Lipases: Application for Si-O Bond Formation and Cleavage
Safety Data Sheet (SDS)
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