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CAS RN: 1487195-87-8 | Product Number: C3165
Cyclopentadienyl(dimethyl fumarate)(triethyl phosphite)cobalt(I)
Purity:
Synonyms:
- [CpCo(dimethyl fumarate)[P(OEt)3]]
Documents:
Size | Unit Price | Hyderabad | Japan* | Quantity |
---|---|---|---|---|
100MG |
₹17,600
|
6 | 15 |
|
*Upon orders receipt, Hyderabad stocks will be dispatched on the same day.
*Items available in Japan warehouse will be dispatched in 10-12 working days.
*INR price is exclusive of domestic taxes applicable.
*TCI frequently reviews storage conditions to optimize them. Please note that the latest information on the storage temperature for the products is described on our website.
Specifications
Appearance | Light yellow to Brown powder to crystal |
Content of Cobalt | 12.8 to 14.3 % |
Properties (reference)
GHS
Pictogram |
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Signal Word | Warning |
Hazard Statements | H351 : Suspected of causing cancer. |
Precautionary Statements | P501 : Dispose of contents/ container to an approved waste disposal plant. P202 : Do not handle until all safety precautions have been read and understood. P201 : Obtain special instructions before use. P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection. P308 + P313 : IF exposed or concerned: Get medical advice/ attention. P405 : Store locked up. |
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Application
Co complex catalyzed [ 2+2+2 ] cycloaddition
The diyne (1 eq.) and catalyst (10 mol %) are weighted into a microwave reaction vial (10 mL) and flushed with argon. Afterward toluene (2-3 mL) and nitrile (5 eq.) are added via syringe and the tube is sealed with a septum. The reaction vessel is introduced to the microwave and heated at 140 °C for 10 min. The solvent is removed under vacuum and the residue charged to silica gel. The crude product is purified on silica gel.
References
- 1)Synthesis of Naphthylpyridines from Unsymmetrical Naphthylheptadiynes and the Configurational Stability of the Biaryl Axis
- 2)Synthesis of Air-Stable and Recyclable CpCoI-Complexes
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